2-[2,2-双-(1H-吲哚-3-基)-乙基]-苯胺合成路线 (共 19 条)
反应条件
SnCl2·2H2O in dichloromethane; water
T=20°C; 72 h;
参考文献
Dupeyre, Gregory; Lemoine, Pascale; Ainseba, Nabila; Michel, Sylvie; Cachet, Xavier
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 22 p. 7780 - 7790
反应条件
tin(II) trifluoromethanesulfonate in dichloromethane
T=40°C;
参考文献
Kinthada, Lakshmana K.; Ghosh, Santanu; De, Subhadip; Bhunia, Subhajit; Dey, Dhananjay; Bisai, Alakesh
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 40 p. 6984 - 6993
反应条件
4-methyl-pent-3-en-2-one; boron trifluoride diethyl etherate; water in dichloromethane
T=0°C; 12 h;
参考文献
Banerji, J.; Saha, R.; Manna, A. Patra'S.; Shoolery, J. N.; Prange, T.; Pascard, C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 2 p. 83 - 87
反应条件
hafnium triflate in acetonitrile
T=20°C; 0.25 h;
参考文献
Aburatani, Sachiko; Uenishi, Jun'ichi
Heterocycles, 2008 , vol. 75, # 6 p. 1407 - 1416
反应条件
potassium methanolate in methanol
6 h; Heating;
参考文献
Bourgeois, Paul; Mesdouze, Jean; Philogene, Emile
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1043 - 1046
反应条件
formic acid
T=20°C; 2 h; Further byproducts given;
参考文献
Somei, Masanori; Yamada, Fumio; Hayashi, Toshikatsu; Goto, Aya; Saga, Yoshitomo
Heterocycles, 2001 , vol. 55, # 3 p. 457 - 460
反应条件
hydrogen; nickel in methanol
Ambient temperature;
参考文献
Ishii, Hisashi; Murakami, Keiko; Sakurada(nee Kawanabe), Eri; Hosoya, Katsuhiro; Murakami, Yasuoki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2377 - 2386
反应条件
1: 0.19 percent / 20 percent H2SO4 / 1 h / Heating
2: 0.82 percent / acetic acid / 2 h / 105 °C
3: 0.04 percent / H2 / Raney Ni / methanol / Ambient temperature
View Scheme
参考文献
Ishii, Hisashi; Murakami, Keiko; Sakurada(nee Kawanabe), Eri; Hosoya, Katsuhiro; Murakami, Yasuoki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2377 - 2386
反应条件
in acetonitrile
T=20°C; 2 h;
参考文献
Aburatani, Sachiko; Uenishi, Jun'ichi
Heterocycles, 2008 , vol. 75, # 6 p. 1407 - 1416
反应条件
1: 87 percent / 24 h
2: d'acide para toluene sulfonique / methanol / 2 h
3: 90 percent / CH3OK / methanol / 6 h / Heating
View Scheme
参考文献
Bourgeois, Paul; Mesdouze, Jean; Philogene, Emile
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1043 - 1046