4-氧代-4-对甲苯基丁酸乙酯合成路线 (共 10 条)
反应条件
formic acid; [Pd(PPh3)2(OAc)2]; tributyl-amine in N,N-dimethyl-formamide T=60°C; 3 h;
参考文献
Arcadi, A.; Cacchi, S.; Marinelli, F.; Misiti, D.
Tetrahedron Letters, 1988 , vol. 29, # 12 p. 1457 - 1460
反应条件
hydrogenchloride T=25°C; 15 h;
参考文献
Kim, Choung Un; Misco, Peter F.; Luh, Bing Y.; Mansuri, Muzammil M.
Tetrahedron Letters, 1994 , vol. 35, # 19 p. 3017 - 3020
反应条件
triethylamine; 1,4-di(diphenylphosphino)-butane; [Rd(cod)OH]2 in 1,4-dioxane; water T=100°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 25 p. 9510 - 9517
反应条件
in N,N-dimethyl-formamide T=160°C; 1 h;
参考文献
Sangu, Kenichiro; Watanabe, Toru; Takaya, Jun; Iwasawa, Nobuharu
Synlett, 2007 , # 6 p. 929 - 933
反应条件
in diethyl ether T=20°C; 1 h;
参考文献
Kashima, Choji; Shirahata, Yoshie; Tsukamoto, Yoshihiro
Heterocycles, 2001 , vol. 54, # 1 p. 309 - 317
反应条件
1: 92 percent / AlCl3 / 1 h / 60 °C 2: 95 percent / HCl / 15 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 19 p. 3017 - 3020
反应条件
tetrakis(triphenylphosphine) palladium(0); zinc copper
参考文献
Chemistry Letters, , # 9 p. 881 - 882
反应条件
1: Br2, AcOH
2: 10 percent / butan-1-ol / Heating
View Scheme
参考文献
Trapani, Giuseppe; Franco, Massimo; Ricciardi, Laura; Latrofa, Andrea; Genchi, Giuseppe; Sanna, Enrico; Tuveri, Francesca; Cagetti, Elisabetta; Biggio, Giovanni; Liso, Gaetano
Journal of Medicinal Chemistry, 1997 , vol. 40, # 19 p. 3109 - 3118
反应条件
sodium ethanolate; benzene
T=40°C;
参考文献
Drake; Adams
Journal of the American Chemical Society, 1939 , vol. 61, p. 1326,1328
反应条件
1: sodium ethylate; benzene / 40 °C
2: benzene
View Scheme
参考文献
Drake; Adams
Journal of the American Chemical Society, 1939 , vol. 61, p. 1326,1328