1,2-BENZ碘XOLE,1,3-二氢-1-羟基-3,3-二甲基合成路线 （共 4 条）
反应条件
potassium hydroxide in dichloromethane; water
3 h;
参考文献
Fernandez Gonzalez, Davinia; Brand, Jonathan P.; Mondiere, Regis; Waser, Jerome
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 8 p. 1631 - 1639
反应条件
1: 56.5 percent / tert-butyl hypochlorite / CCl4 / 0.5 h
2: 53 percent / aq. KOH / CH2Cl2 / 0.33 h
View Scheme
参考文献
Moss, Robert A.; Wilk, Boguslawa; Krogh-Jespersen, Karsten; Blair, John T.; Westbrook, John D.
Journal of the American Chemical Society, 1989 , vol. 111, # 1 p. 250 - 258
反应条件
potassium hydroxide in dichloromethane
T=20°C;
参考文献
Geary, Gemma C.; Hope, Eric G.; Singh, Kuldip; Stuart, Alison M.
Chemical Communications, 2013 , vol. 49, # 81 p. 9263 - 9265
反应条件
1: 73 percent / diethyl ether / 1 h / Heating
2: 56.5 percent / tert-butyl hypochlorite / CCl4 / 0.5 h
3: 53 percent / aq. KOH / CH2Cl2 / 0.33 h
View Scheme
参考文献
Moss, Robert A.; Wilk, Boguslawa; Krogh-Jespersen, Karsten; Blair, John T.; Westbrook, John D.
Journal of the American Chemical Society, 1989 , vol. 111, # 1 p. 250 - 258
