1-(甲硫基)丙-2-醇合成路线 (共 18 条)
反应条件
dihydrogen peroxide in acetic acid
参考文献
Alcudia,F. et al.
Canadian Journal of Chemistry, 1979 , vol. 57, # 18 p. 2426 - 2433
反应条件
in chlorobenzene Kinetics;
参考文献
Malievskii
Petroleum Chemistry, 2012 , vol. 52, # 3 p. 194 - 203
反应条件
sodium hydroxide in methanol
T=20°C; 2 h;
参考文献
Jain, Monish; Fan, Junying; Baturay, Nesrine Z.; Kwon, Chul-Hoon
Journal of Medicinal Chemistry, 2004 , vol. 47, # 15 p. 3843 - 3852
反应条件
triethylamine
T=100°C;
参考文献
Marvel; Weil
Journal of the American Chemical Society, 1954 , vol. 76, p. 61,67
参考文献
Rhone-Poulenc Sante
Patent: US5008280 A1, 1991 ;
反应条件
n-butyllithium; naphthalenyllithium in tetrahydrofuran; diethyl ether
-78 deg C, 2 h; to 20 deg C, overnight;
参考文献
Barluenga, Jose; Florez, Josefa; Yus, Miguel
Journal of the Chemical Society, Chemical Communications, 1982 , # 20 p. 1153 - 1154
参考文献
Bordwell; Andersen
Journal of the American Chemical Society, 1953 , vol. 75, p. 4959,4961
参考文献
Hunt; Marvel
Journal of the American Chemical Society, 1935 , vol. 57, p. 1696
Journal of the American Chemical Society, 1936 , vol. 58, p. 2659
反应条件
sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide
1.) THF, 25 deg C, overnight, 2.) 1 h; Multistep reaction;
参考文献
Nelson, Donna J.; Cooper, Penny J.; Soundararajan, Raman
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1414 - 1418
反应条件
in tetrahydrofuran; diethyl ether
T=-78 - 20°C; 12 h; Yield given;
参考文献
Barluenga, Jose; Fananas, Francisco J.; Villamana, Jorge; Yus, Miguel
Journal of Organic Chemistry, 1982 , vol. 47, # 8 p. 1560 - 1564