1-(甲硫基)丙-2-醇合成路线 （共 18 条）
反应条件
lithium aluminium tetrahydride
参考文献
Huyser,E.S.; Kellogg,R.M.
Journal of Organic Chemistry, 1966 , vol. 31, p. 3366 - 3369
参考文献
Prochazka,M.; Durdovic,P.
Collection of Czechoslovak Chemical Communications, 1977 , vol. 42, p. 2401 - 2407
反应条件
n-butyllithium
1) THF, hexane, -78 deg C, 1 h; 2) THF, hexane, rt, 2 h; Yield givenMultistep reaction;
参考文献
Fromont, Christophe; Masson, Serge
Tetrahedron, 1999 , vol. 55, # 17 p. 5405 - 5418
反应条件
lithium biphenylide
1) THF, -80 deg C, 1 h, 2) THF, -80 deg C to RT; Yield given. Multistep reaction;
参考文献
Bartmann, Ekkehard
Angewandte Chemie, 1986 , vol. 98, # 7 p. 629 - 631
反应条件
sodium hydroxide; sodium tetrahydroborate; mercury(II) diacetate
Yield given. Multistep reaction;
参考文献
Brown, Herbert C.; Lynch, Gary J.
Journal of Organic Chemistry, 1981 , vol. 46, # 5 p. 930 - 939
参考文献
Bordwell; Andersen
Journal of the American Chemical Society, 1953 , vol. 75, p. 4959,4961
反应条件
in tetrahydrofuran; diethyl ether
T=-78 - 20°C; reaction with other electrophiles; reaction of organolithium compounds formed from chlorohydrins with various electrophiles (D2O, O2, CO2, PhCH2Br, Me2S2, carbonyl compounds); Product distribution;
参考文献
Barluenga, Jose; Florez, Josefa; Yus, Miguel
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 3019 - 3026
反应条件
potassium hydroxide
T=220 - 250°C;
参考文献
Prochazka,M.; Durdovic,P.
Collection of Czechoslovak Chemical Communications, 1977 , vol. 42, p. 2401 - 2407
