NaOH; acid in water
free acid ligand was dissolved in dilute aq. NaOH, adjusted with diluteacid to pH 6-7; prepd. soln. was filterted and added to aq. soln. of metal acetate; filtration, washing, air drying; elem. anal.;
参考文献
Albanese, N. F.; Haendler, H. M.
Polyhedron, 1983 , vol. 2, p. 1131 - 1140
in ethanol
addn. of NH4OH to the Ni compd. under N2 and addn. of o-aminobenzoic acid in EtOH to the pptd. hydroxide; filtn. and washing twice with EtOH; elem. anal.;
参考文献
Vithal, M.; Babu, T. G. Narendra; Murthy, B. Narsimha
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1989 , vol. 28, p. 689 - 692
in ethanol
addn. of NH4OH to the Ni compd. under N2 and addn. of o-aminobenzoic acid in EtOH to the pptd. hydroxide; filtn. and washing twice with EtOH; elem. anal.;
参考文献
Vithal, M.; Babu, T. G. Narendra; Murthy, B. Narsimha
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1989 , vol. 28, p. 689 - 692
Feigl, F.; Miranda, L. I.; Spinelli, H. A.
Min. Agr. Dept. Nacl. Prod. Mineral Lab. Prod. Mineral (Brazil, 1943 , vol. 11, p. 79 - 95
C.A., 1946 , p. 3427