1-O-苯甲酰基-1,3-丙烷二醇合成路线 （共 25 条）
反应条件
oxygen; potassium carbonate
T=30°C; 24 h;
参考文献
Yasukawa, Tomohiro; Miyamura, Hiroyuki; Kobayashi, Shu
Chemistry - An Asian Journal, 2011 , vol. 6, # 2 p. 621 - 627
反应条件
hydrogen; palladium on activated charcoal
Yield given;
参考文献
Mukaiyama, Teruaki; Ohshima, Masahiro; Nagaoka, Hitoshi; Murakami, Masahiro
Chemistry Letters, 1984 , p. 615 - 618
反应条件
1: 83 percent / 4-dimethylaminopyridine, pyridine / 0 °C
2: 88 percent / AlCl3, PhNMe2 / CH2Cl2 / 1 h / Ambient temperature
View Scheme
参考文献
Akiyama, Takahiko; Hirofuji, Hajimu; Ozaki, Shoichiro
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 7 p. 1932 - 1938
反应条件
aluminum oxide; oxone in chloroform
T=50°C; 2 h; Product distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Akbalina; Zlotskii; Kabal'nova; Grigor'ev; Kotlyar; Shereshovets
Russian Journal of Applied Chemistry, 2002 , vol. 75, # 7 p. 1120 - 1122
反应条件
aluminum oxide; methanesulfonic acid
T=80°C; 0.5 h;
参考文献
Sharghi, Hashem; Sarvari, Mona Hosseini
Tetrahedron, 2003 , vol. 59, # 20 p. 3627 - 3633
反应条件
1: tetra-n-butylammonium tribromide; trimethyl orthoformate / acetonitrile / 20 °C
2: water / acetonitrile-D3 / 3.33 h / UV-irradiation
View Scheme
参考文献
Thevenet, Damien; Neier, Reinhard
Helvetica Chimica Acta, 2011 , vol. 94, # 2 p. 331 - 346
反应条件
(CH3)2SnCl; potassium carbonate in tetrahydrofuran
12 h; varying amount of reag.; Product distribution;
参考文献
Maki, Toshihide; Iwasaki, Fumiaki; Matsumura, Yoshihiro
Tetrahedron Letters, 1998 , vol. 39, # 31 p. 5601 - 5604
反应条件
IPrCO2
T=120°C; 3 h; Inert atmosphere;
参考文献
Wang, Yanqin; Li, Zhenjiang
Chinese Journal of Catalysis, 2012 , vol. 33, # 2-3 p. 502 - 507
参考文献
Paterson, Ian; Smith, Julian D.
Tetrahedron Letters, 1993 , vol. 34, # 33 p. 5351 - 5354
参考文献
Rovira; Halasz
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1941 , vol. 212, p. 643
