5-(4-甲氧基苯基)-3-(甲基硫代)-1,2,4-三嗪合成路线 （共 4 条）
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene
T=20°C; 1 h;
参考文献
Alphonse, France-Aimee; Suzenet, Franck; Keromnes, Anne; Lebret, Bruno; Guillaumet, Gerald
Synthesis, 2004 , # 17 p. 2893 - 2899
反应条件
sodium hydrogencarbonate in ethanol
T=0°C; 4 h;
参考文献
Taylor, C. Edward; Pont, Joseph L.; Warner, John C.
Tetrahedron, 1987 , vol. 43, # 21 p. 5159 - 5168
反应条件
sodium carbonate in ethanol; water
T=0°C; 6 h;
参考文献
Pellegatti, Laurent; Vedrenne, Emeline; Leger, Jean-Michel; Jarry, Christian; Routier, Sylvain
Tetrahedron, 2010 , vol. 66, # 24 p. 4383 - 4389
反应条件
1: 85 percent / tetrahydrofuran / 20 h / 20 °C
2: 100 percent / DDQ / toluene / 1 h / 20 °C
View Scheme
参考文献
Alphonse, France-Aimee; Suzenet, Franck; Keromnes, Anne; Lebret, Bruno; Guillaumet, Gerald
Synthesis, 2004 , # 17 p. 2893 - 2899
