1,4,7,10,13-戊氧杂环十六烷-15-醇合成路线 (共 2 条)
反应条件
1: t-BuONa / 2-methyl-propan-2-ol / 2 h / 60 °C
2: 0.23 g / H2, p-toluenesulfonic acid / Pd/C
View Scheme
参考文献
Ikeda; Katayama; Tsuchiya; Okahara
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2473 - 2475
反应条件
sodium hydride
1.) dioxane, 2.) dioxane, a) 40 deg C, 1 h, b) 60 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Ikeda; Katayama; Tsuchiya; Okahara
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2473 - 2475