3-chloroprop-1-ene; trifluoroacetic acid; zinc; Co(2,2'-bipyridine)Br2 in pyridine; N-dodecane; acetonitrile T=50°C; 8 h; Title compound not separated from byproducts;
palladium diacetate; triphenylphosphine on polystyrene in tetrahydrofuran T=120°C; 1.5 h;
参考文献
Srivastava, Rajiv R.; Zych, Andrew J.; Jenkins, David M.; Wang, Hong-Jun; Chen, Zhen-Jia; Fairfax, David J.
Synthetic Communications, 2007 , vol. 37, # 3 p. 431 - 438