反应条件
H2CCHI in dimethyl sulfoxide Irradiation (UV/VIS); mercurial and organic compound dissolved in nitrogen purged solvent, irradn. (350-nm Rayonet photoreactor, 35-40°C, 12h);; mixt. poured into water; extn. with benzene; ext. washed (aq. Na2S2O3), dried (Na2SO4) and concd. (vacuum); yield detd. by GLC;;
参考文献
Journal of the American Chemical Society, , vol. 110, # 11 p. 3530 - 3538