2-氨基-4-甲基吡啶合成路线 (共 193 条)
反应条件
1: dicyclohexyl-carbodiimide / dichloromethane / 20 °C
2: copper(l) iodide; 1,10-phenanthroline; potassium acetate; tetrabutylammomium bromide / N,N-dimethyl-formamide / 5 h / 100 °C
View Scheme
参考文献
Sun, Jie; Tan, Qitao; Yang, Wusong; Liu, Bingxin; Xu, Bin
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 2-3 p. 388 - 394
反应条件
copper; potassium carbonate
T=190°C; 2 h; Yield given;
参考文献
Wintersteiger, Reinhold; Wolfbeis, Otto S.
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1983 , vol. 38, # 2 p. 248 - 250
参考文献
Elghamry, Ibrahim
Synthetic Communications, 2009 , vol. 39, # 17 p. 3010 - 3015
参考文献
Elghamry, Ibrahim
Synthetic Communications, 2009 , vol. 39, # 17 p. 3010 - 3015
反应条件
copper(l) iodide; boron trifluoride diethyl etherate; oxygen in neat (no solvent)
T=40°C; P=760.051 Torr; 24 h; Schlenk technique;
参考文献
Cai, Zhong-Jian; Wang, Shun-Yi; Ji, Shun-Jun
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 13 p. 2686 - 2692
反应条件
anhydrous iron chloride
T=90°C; 4 h;
参考文献
Yan, Hao; Wang, Yuling; Pan, Congming; Zhang, Hao; Yang, Sizhuo; Ren, Xiaoyu; Li, Jian; Huang, Guosheng
European Journal of Organic Chemistry, 2014 , vol. 2014, # 13 p. 2754 - 2763
参考文献
Ohkata, Katsuo; Ohsugi, Minoru; Yamamoto, Kazuhiro; Ohsawa, Mika; Akiba, Kin-Ya
Journal of the American Chemical Society, 1996 , vol. 118, # 27 p. 6355 - 6369
反应条件
1: Et3N / 2 h / Heating
2: CH2Cl2 / 0 °C
3: 86 percent / toluene / Heating
View Scheme
参考文献
Ohkata, Katsuo; Ohsugi, Minoru; Yamamoto, Kazuhiro; Ohsawa, Mika; Akiba, Kin-Ya
Journal of the American Chemical Society, 1996 , vol. 118, # 27 p. 6355 - 6369
反应条件
sulfur in ethanol
24 h; Heating;
参考文献
Sudha, L. V.; Manogaran, S.; Sathyanarayana, D. N.
Magnetic Resonance in Chemistry, 1985 , vol. 23, # 7 p. 591 - 596
参考文献
Capitan-Vallvey, L. F.; Salinas, F.; Jimenez, C.; Cuadros, L.
Canadian Journal of Chemistry, 1982 , vol. 60, p. 1706 - 1712