1: 1-hydroxy-3-methyl-2,5-dihydro-1H-phosphole 1-oxide With 1-propanephosphonic acid cyclic anhydride in ethyl acetate
0.166667 h; Green chemistry;
2: methanol in ethyl acetate
T=25°C; 0.5 h; Green chemistry;
Arbuzov, B. A.; Vizel', A. O.; Shchukina, L. I.; Vakulenko, O. V.; Zyablikova, T. A.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1705 - 1709,1514 - 1518
Arbuzov, B. A.; Vizel', A. O.; Shchukina, L. I.; Vakulenko, O. V.; Zyablikova, T. A.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1705 - 1709,1514 - 1518
1: 65 percent / diethyl ether / -45 to -40 deg C, then r.t.
2: 68 percent / 1 h / 100 - 110 °C
View Scheme
参考文献
Arbuzov, B. A.; Vizel', A. O.; Shchukina, L. I.; Vakulenko, O. V.; Zyablikova, T. A.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1705 - 1709,1514 - 1518
Berestovitskaya, V. M.; Efremov, D. A.; Berkova, G. A.; Perekalin, V. V.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 11 p. 2418 - 2428,2084 - 2092
Arbuzov, B. A.; Vizel', A. O.; Shchukina, L. I.; Giniyatullin, R. S.
Doklady Chemistry, 1980 , vol. 253, p. 371 - 374
Dokl. Akad. Nauk SSSR Ser. Khim., 1980 , vol. 253, # 4 p. 879 - 883
methanol
2 h; Heating; Yield given. Yields of byproduct given;
参考文献
Arbuzov, B. A.; Vizel', A. O.; Shchukina, L. I.; Giniyatullin, R. S.
Doklady Chemistry, 1980 , vol. 253, p. 371 - 374
Dokl. Akad. Nauk SSSR Ser. Khim., 1980 , vol. 253, # 4 p. 879 - 883
