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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6950-01-2
合成路线
(共 17 条)
104014-43-9
→
反应条件
6950-01-2
反应条件
pyridine; oxygen; cupric trifluoroacetate in N,N-dimethyl-formamide T=130°C; P=760.051 Torr; 48 h; Schlenk technique;
参考文献
Yu, Jipan; Yang, Haijun; Jiang, Yuyang; Fu, Hua
Chemistry - A European Journal, 2013 , vol. 19, # 13 p. 4271 - 4277
83060-84-8
→
反应条件
6950-01-2
反应条件
anhydrous heptafluorobutyric acid Heating;
参考文献
Iwao, M.; Reed, J. N.; Snieckus, V.
Journal of the American Chemical Society, 1982 , vol. 104, # 20 p. 5531 - 5533
107772-63-4
→
反应条件
6950-01-2
反应条件
phosphorous pentoxide; phosphoric acid T=110°C; Friedel Crafts acylation; 16 h;
参考文献
Deiters, Emmanuel; Gumy, Frederic; Buenzli, Jean-Claude G.
European Journal of Inorganic Chemistry, 2010 , # 18 p. 2723 - 2734
536-90-3
间氨基苯甲醚
→
反应条件
6950-01-2
反应条件
1: K2CO3 / copper / 3-methyl-butan-1-ol / 10 h / 160 °C 2: H3PO4; P2O5 / 3 h / 110 °C View Scheme
参考文献
Boumendjel, Ahcene; Macalou, Sira; Ahmed-Belkacem, Abdelhakim; Blanc, Madeleine; Di Pietro, Attilio
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 8 p. 2892 - 2897
118-91-2
2-氯苯甲酸
→
反应条件
6950-01-2
反应条件
1: K2CO3 / copper / 3-methyl-butan-1-ol / 10 h / 160 °C 2: H3PO4; P2O5 / 3 h / 110 °C View Scheme
参考文献
Boumendjel, Ahcene; Macalou, Sira; Ahmed-Belkacem, Abdelhakim; Blanc, Madeleine; Di Pietro, Attilio
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 8 p. 2892 - 2897
27693-73-8
→
反应条件
6950-01-2
反应条件
phosphoric acid; phosphorus pentoxide T=110°C; 3 h;
参考文献
Boumendjel, Ahcene; Macalou, Sira; Ahmed-Belkacem, Abdelhakim; Blanc, Madeleine; Di Pietro, Attilio
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 8 p. 2892 - 2897
137654-21-8
2-(2-二甲胺乙基)-5-甲基-吡唑-3-基胺
→
反应条件
6950-01-2
反应条件
1: sodium amide / tetrahydrofuran / 16 h / 50 °C 2: phosphorous pentoxide; phosphoric acid / 16 h / 110 °C View Scheme
参考文献
Deiters, Emmanuel; Gumy, Frederic; Buenzli, Jean-Claude G.
European Journal of Inorganic Chemistry, 2010 , # 18 p. 2723 - 2734
74497-02-2
→
反应条件
6950-01-2
反应条件
1: sodium amide / tetrahydrofuran / 16 h / 50 °C 2: phosphorous pentoxide; phosphoric acid / 16 h / 110 °C View Scheme
参考文献
Deiters, Emmanuel; Gumy, Frederic; Buenzli, Jean-Claude G.
European Journal of Inorganic Chemistry, 2010 , # 18 p. 2723 - 2734
445-29-4
邻氟苯甲酸
→
反应条件
6950-01-2
反应条件
1: sodium amide / tetrahydrofuran / 16 h / 50 °C 2: phosphorous pentoxide; phosphoric acid / 16 h / 110 °C View Scheme
参考文献
Deiters, Emmanuel; Gumy, Frederic; Buenzli, Jean-Claude G.
European Journal of Inorganic Chemistry, 2010 , # 18 p. 2723 - 2734
27693-73-8
→
反应条件
61736-68-3
乳化剂MOA-3,7,9,15,20
+
6950-01-2
反应条件
phosphorous pentoxide; phosphoric acid T=110°C; Friedel Crafts acylation; 16 h;
参考文献
Deiters, Emmanuel; Gumy, Frederic; Buenzli, Jean-Claude G.
European Journal of Inorganic Chemistry, 2010 , # 18 p. 2723 - 2734
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