3-O-叔丁基二甲基甲硅烷基腺苷酸合成路线 (共 3 条)
反应条件
ammonium cerium(IV) nitrate; silica gel in tetrachloromethane; isopropyl alcohol
desilylation; 9 h; Heating;
参考文献
Hwu, Jih Ru; Jain, Moti L.; Tsai, Fu-Yuan; Tsay, Shwu-Chen; Balakumar, Arumugham; Hakimelahi, Gholam H.
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5077 - 5088
反应条件
methanol; formic acid
T=5 - 20°C; Inert atmosphere; chemoselective reaction;
参考文献
Chandra, Tilak; Broderick, William E.; Broderick, Joan B.
Nucleosides, Nucleotides and Nucleic Acids, 2009 , vol. 28, # 11-12 p. 1016 - 1029
反应条件
in methanol
T=30°C; half time of isomerisation; Rate constant;
参考文献
Ogilvie, Kelvin K.; Entwistle, Douglas W.
Carbohydrate Research, 1981 , vol. 89, p. 203 - 210