1,3,4,6-O-四乙酰基-2-脱氧-D-吡喃葡萄糖合成路线 （共 3 条）
反应条件
1: hydrogen bromide / dichloromethane / 96 h / 20 °C / Inert atmosphere 2: 1-methyl-1H-imidazole; zinc / ethyl acetate / 18 h / Reflux; Inert atmosphere View Scheme
参考文献
Wolf, Saskia; Berrio, Rosmirt Molina; Meier, Chris
European Journal of Organic Chemistry, 2011 , # 31 p. 6304 - 6313
反应条件
1: 5.2 percent / SnCl4 / CH2Cl2 / 0.75 h / 60 - 70 °C
2: 66.3 percent / sat. methanol. NH3 / 0 °C
View Scheme
参考文献
Sakaguchi, Masakazu; Larroquette, Cynthia A.; Agrawal, Krishna C.
Journal of Medicinal Chemistry, 1983 , vol. 26, # 1 p. 20 - 24
反应条件
1: 15.1 percent / SnCl4 / CH2Cl2 / 0.75 h / 60 - 70 °C
2: 95.4 percent / sat. methanol. NH3 / 0 °C
View Scheme
参考文献
Sakaguchi, Masakazu; Larroquette, Cynthia A.; Agrawal, Krishna C.
Journal of Medicinal Chemistry, 1983 , vol. 26, # 1 p. 20 - 24
