2-(4-甲氧基苯基)-1,3,2-二氧硼戊环合成路线 (共 7 条)
反应条件
potassium phosphate; hydroquinone; tri-cyclo-hexyl-phosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=70°C;
参考文献
Lu, Ting-Yi; Xue, Cuihua; Luo, Fen-Tair
Tetrahedron Letters, 2003 , vol. 44, # 8 p. 1587 - 1590
反应条件
tri-ruthenium(0)dodecacarbonyl in toluene T=140°C; 20 h;
参考文献
Tatamidani, Hiroto; Yokota, Kazuhiko; Kakiuchi, Fumitoshi; Chatani, Naoto
Journal of Organic Chemistry, 2004 , vol. 69, # 17 p. 5615 - 5621
反应条件
1: 1-bromo-4-methoxy-benzene With magnesium in tetrahydrofuran
2: With boric acid trimethyl ester in tetrahydrofuran
T=-78 - 20°C;
3: ethylene glycol in toluene
Heating; Further stages.;
参考文献
Wong, Ken-Tsung; Chien, Yuh-Yih; Liao, Yuan-Li; Lin, Chang-Chih; Chou, Meng-Yen; Leung, Man-Kit
Journal of Organic Chemistry, 2002 , vol. 67, # 3 p. 1041 - 1044
反应条件
potassium carbonate; palladium diacetate in water; acetone
T=65°C; 0.67 h;
参考文献
Wallow, Thomas I.; Novak, Bruce M.
Journal of Organic Chemistry, 1994 , vol. 59, # 17 p. 5034 - 5037
反应条件
potassium carbonate; palladium diacetate in water; acetone
T=65°C; 16 h;
参考文献
Wallow, Thomas I.; Novak, Bruce M.
Journal of Organic Chemistry, 1994 , vol. 59, # 17 p. 5034 - 5037
反应条件
potassium carbonate; palladium diacetate in water; acetone
T=65°C; 0.67 h;
参考文献
Wallow, Thomas I.; Novak, Bruce M.
Journal of Organic Chemistry, 1994 , vol. 59, # 17 p. 5034 - 5037
反应条件
potassium carbonate; palladium diacetate in water; acetone
T=65°C; 4 h; Yield given;
参考文献
Wallow, Thomas I.; Novak, Bruce M.
Journal of Organic Chemistry, 1994 , vol. 59, # 17 p. 5034 - 5037