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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
间溴苯腈
合成路线
（共 176 条）
6952-59-6
间溴苯腈
→
反应条件
36852-02-5
联苯-3,3-二甲腈
+
100-47-0
苯甲腈
反应条件
1: With chloro-trimethyl-silane; ethylene dibromide; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; lithium chloride; cobalt(II) chloride; zinc in tetrahydrofuran T=20°C; 35 h; Inert atmosphere; 2: With iodine in tetrahydrofuran 0.5 h;
参考文献
Jin, Meng-Yi; Yoshikai, Naohiko
Journal of Organic Chemistry, 2011 , vol. 76, # 7 p. 1972 - 1978
6952-59-6
间溴苯腈
+
31268-20-9
+
128796-39-4
4-三氟甲基苯硼酸
→
反应条件
反应条件
palladium diacetate; cesium fluoride; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran T=65°C; Suzuki-Miyaura reaction; 5 h; Inert atmosphere;
参考文献
Mollar, Cristian; Besora, Maria; Maseras, Feliu; Asensio, Gregorio; Medio-Simon, Mercedes
Chemistry - A European Journal, 2010 , vol. 16, # 45 p. 13390 - 13397
6952-59-6
间溴苯腈
+
107-19-7
2-丙炔-1-醇
→
反应条件
170859-72-0
3-(3-羟基-1-丙炔基)-苯甲腈
反应条件
pyridine; copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride T=75°C; 6 h;
参考文献
Dulog, Lothar; Koerner, Bernd; Heinze, Juergen; Yang, Jianjun
Liebigs Annalen, 1995 , # 9 p. 1663 - 1672
6952-59-6
间溴苯腈
+
31268-20-9
+
5720-07-0
→
反应条件
71426-20-5
+
154197-00-9
反应条件
palladium diacetate; cesium fluoride; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran T=65°C; Suzuki-Miyaura reaction; 5 h; Inert atmosphere;
参考文献
Mollar, Cristian; Besora, Maria; Maseras, Feliu; Asensio, Gregorio; Medio-Simon, Mercedes
Chemistry - A European Journal, 2010 , vol. 16, # 45 p. 13390 - 13397
6952-59-6
间溴苯腈
→
反应条件
725228-49-9
反应条件
1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 - 20 °C / Inert atmosphere 1.2: 0 °C / Reflux 2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / acetonitrile; water / 1 h / 90 °C 3.1: sodium tetrahydroborate / NiII chloride hexahydrate / methanol / 0 - 20 °C / Cooling with ice 4.1: hydrogen / palladium-on-charcoal / methanol / 1 h View Scheme
参考文献
CORNELL UNIVERSITY; COFERON, INC.; PURDUE RESEARCH FOUNDATION
Patent: US2012/295874 A1, 2012 ;
US 20120295874 A1
108-22-5
+
6952-59-6
间溴苯腈
→
反应条件
73013-50-0
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-n-butyltin methoxide; N-[2'-(dicyclohexylphosphino)-1,1'-biphenyl-2-yl]-N,N-dimethylamine in toluene T=100°C;
参考文献
Liu, Ping; Lanza Jr., Thomas J.; Jewell, James P.; Jones, Carrie P.; Hagmann, William K.; Lin, Linus S.
Tetrahedron Letters, 2003 , vol. 44, # 49 p. 8869 - 8871
6952-59-6
间溴苯腈
→
反应条件
76650-08-3
反应条件
1.1: iodine; magnesium / diethyl ether / Inert atmosphere 1.2: 6 h / Reflux 1.3: Heating 2.1: bromine / diethyl ether / 20 °C / Cooling with ice View Scheme
参考文献
Lagoja, Irene; Pannecouque, Christophe; Griffioen, Gerard; Wera, Stefaan; Rojasdelaparra, Veronica Maria; Van Aerschot, Arthur
European Journal of Pharmaceutical Sciences, 2011 , vol. 43, # 5 p. 386 - 392
6952-59-6
间溴苯腈
→
反应条件
773060-41-6
反应条件
1: piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) / 1 h / 65 °C 2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h View Scheme
参考文献
Seltmann, Jens; Mueller, Kathrin; Klein, Susanne; Lehmann, Matthias
Chemical Communications, 2011 , vol. 47, # 23 p. 6680 - 6682
6952-59-6
间溴苯腈
+
57260-71-6
→
反应条件
807624-20-0
反应条件
1: With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate in xylene T=50°C; 2: With macroporous polymer-supported isocyanate in xylene T=50°C; 24 h;
参考文献
Duncton, Matthew A. J.; Roffey, Jonathan R. A.; Hamlyn, Richard J.; Adams, David R.
Tetrahedron Letters, 2006 , vol. 47, # 15 p. 2549 - 2552
1450-14-2
+
6952-59-6
间溴苯腈
→
反应条件
82142-18-5
反应条件
potassium fluoride; tris-(dibenzylideneacetone)dipalladium(0); biphenyl-2-yl-di-tert-butyl-phosphane in various solvent(s) T=100°C; Substitution; silylation;
参考文献
Goossen; Ferwanah
Synlett, 2000 , # 12 p. 1801 - 1803
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