您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
间溴苯腈
合成路线
（共 176 条）
6952-59-6
间溴苯腈
+
124-38-9
二氧化碳
→
反应条件
1877-72-1
3-氰基苯甲酸
反应条件
1: meta-bromobenzonitrile With n-butyllithium in tetrahydrofuran T=-70°C; 0.25 h; 2: carbon dioxide in tetrahydrofuran; diethyl ether Further stages.;
参考文献
Lulinski, Sergiusz; Zajac, Katarzyna
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7785 - 7788
6952-59-6
间溴苯腈
+
201230-82-2
→
反应条件
1877-72-1
3-氰基苯甲酸
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide; bis(benzonitrile)palladium(II) dichloride; triphenylphosphine in xylene T=90°C; Carbonylation; 4 h;
参考文献
Lapidus; Petrovskii; Bruk; Beletskaya
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 11 p. 1636 - 1639
6952-59-6
间溴苯腈
+
68-12-2
N,N-二甲基甲酰胺
→
反应条件
626-17-5
间苯二甲腈
反应条件
1: With magnesium in tetrahydrofuran T=20°C; 2: With ammonia; iodine in tetrahydrofuran; water T=20°C;
参考文献
Ishii, Genki; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron Letters, 2011 , vol. 52, # 18 p. 2404 - 2406
6952-59-6
间溴苯腈
→
反应条件
626-17-5
间苯二甲腈
反应条件
1: With isopropylmagnesium chloride; lithium chloride in tetrahydrofuran T=-15°C; 0.25 h; 2: With N,N-dimethyl-formamide in tetrahydrofuran T=0°C; 2 h; 3: With ammonia; iodine in tetrahydrofuran; water T=20°C; 2 h;
参考文献
Ishii, Genki; Harigae, Ryo; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2013 , vol. 69, # 5 p. 1462 - 1469
6952-59-6
间溴苯腈
+
917-54-4
甲基锂
→
反应条件
74702-93-5
1-(3-溴苯基)-1-甲基乙胺
反应条件
1: methyllithium With cerium(III) chloride in tetrahydrofuran; diethyl ether 0.5 h; Cooling with acetone-dry ice; 2: meta-bromobenzonitrile in tetrahydrofuran; diethyl ether
参考文献
ALBANY MOLECULAR RESEARCH, INC.
Patent: WO2010/132437 A1, 2010 ;
Location in patent: Page/Page column 70; 115-116 ;
WO 2010/132437 A1
6952-59-6
间溴苯腈
→
反应条件
69113-59-3
间碘苯腈
反应条件
KI-CuI-alumina in various solvent(s) T=150°C; 4 h; other reagents; Product distribution;
参考文献
Clark, James H.; Jones, Craig W.; Duke, Catherine V. A.; Miller, Jack M.
Journal of Chemical Research, Miniprint, 1989 , # 8 p. 1745 - 1758
6952-59-6
间溴苯腈
+
75-36-5
乙酰氯
→
反应条件
6136-68-1
3-乙酰苯腈
反应条件
1: meta-bromobenzonitrile With ethylene dibromide; zinc in acetonitrile T=20°C; Electrochemical reaction; 2: acetyl chloride in acetonitrile T=20°C;
参考文献
Fillon, Hyacinthe; Gosmini, Corinne; Perichon, Jacques
Tetrahedron, 2003 , vol. 59, # 41 p. 8199 - 8202
6952-59-6
间溴苯腈
+
108-24-7
乙酸酐
→
反应条件
6136-68-1
3-乙酰苯腈
反应条件
3-chloroprop-1-ene; cobalt(II) dibromide; zinc; trifluoroacetic acid in acetonitrile 24 h;
参考文献
Kazmierski, Igor; Bastienne, Mylene; Gosmini, Corinne; Paris, Jean-Marc; Perichon, Jacques
Journal of Organic Chemistry, 2004 , vol. 69, # 3 p. 936 - 942
6952-59-6
间溴苯腈
→
反应条件
6136-68-1
3-乙酰苯腈
反应条件
1: 1,3-bis(diphenylphosphino)propane; Pd(OAc)2; Et3N / 1-butyl-3-methylimidazolium tetrafluoroborate / 36 h / 115 °C 2: aq. HCl / 0.5 h View Scheme
参考文献
Cabri, Walter; Candiani, Ilaria; Bedeschi, Angelo; Penco, Sergio; Santi, Roberto
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1481 - 1486
6952-59-6
间溴苯腈
+
75-05-8
乙腈
→
反应条件
70591-86-5
3-溴苯酰乙腈
反应条件
1: With sodium hydride; tert-butyl alcohol in tetrahydrofuran T=40°C; 8 h; 2: With hydrogenchloride in chloroform T=20°C; 4 h;
参考文献
Takayama, Kazuhisa; Iwata, Masahiro; Hisamichi, Hiroyuki; Okamoto, Yoshinori; Aoki, Motonori; Niwa, Akira
Chemical and pharmaceutical bulletin, 2002 , vol. 50, # 8 p. 1050 - 1059
首页
上一页
1
2
3
4
5
6
7
8
...
18
下一页
末页
到第
页
确定
