反应条件
1: diethyl ether / 1 h / Ambient temperature
2: 1.) borane, 2.) CsF, sodium carbonate / 1.) THF, RT, 16 h, 2.) EtOH, reflux, 16 h
3: 99 percent / H2 / 10percent Pd/C / ethanol / 6 h / 2280 Torr
View Scheme
参考文献
Macor; Post; Ryan
Synthetic Communications, 1993 , vol. 23, # 1 p. 65 - 72