9,10-二氢-2,7-二硝基-菲合成路线 （共 5 条）
反应条件
sulfuric acid; nitric acid; acetic acid; acetic anhydride
T=0 - 20°C; 24 h;
参考文献
Nelsen, Stephen F.; Luo, Yun; Weaver, Michael N.; Lockard, Jenny V.; Zink, Jeffrey I.
Journal of Organic Chemistry, 2006 , vol. 71, # 11 p. 4286 - 4295
反应条件
nitric acid; acetic acid
T=0 - 5°C; 6 h;
参考文献
Eirin, Ana; Fernandez, Franco; Gomez, Generosa; Lopez, Carmen; Santos, Ana; Rodriguez, Gonzalo
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1994 , vol. 336, # 1 p. 63 - 66
反应条件
nitric acid in acetic anhydride
T=5°C; 24 h; var. solvents, temp., reaction time, and HNO3 concentration;
参考文献
Fernandez, Franco; Lerma, J. Lopez De; Perales, Aurea; Rodriguez, Gonzalo
Journal of Chemical Crystallography, 1994 , vol. 24, # 7 p. 451 - 456
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane
3 h; Heating;
参考文献
Nimura; Kikuchi; Ohana; Yabe; Kondo; Kaise
Journal of Physical Chemistry A, 1997 , vol. 101, # 11 p. 2083 - 2088
反应条件
1: 50 percent / NBS, (PhCOO)2 / CCl4 / 3 h / Heating
2: 72 percent / SnCl2, H2O, HCl / acetic acid / 0.05 h
View Scheme
参考文献
Nimura; Kikuchi; Ohana; Yabe; Kondo; Kaise
Journal of Physical Chemistry A, 1997 , vol. 101, # 11 p. 2083 - 2088
