氯代三叔丁基磷化金(I)合成路线 （共 10 条）
反应条件
phloroglucinol trimethyl ether in 1,2-dichloro-ethane T=150°C; 22 h; Inert atmosphereSchlenk technique; Reagent/catalyst;
参考文献
Tetrahedron, , vol. 69, # 27-28 p. 5751 - 5757
反应条件
in 1,2-dichloro-ethane T=150°C; 22 h; Inert atmosphereSchlenk technique;
参考文献
Tetrahedron, , vol. 69, # 27-28 p. 5751 - 5757
反应条件
in dichloromethane 1.75 h;
参考文献
Hashmi, A. Stephen K.; Bechem, Benjamin; Loos, Annette; Hamzic, Melissa; Rominger, Frank; Rabaa, Hassan
Australian Journal of Chemistry, 2014 , vol. 67, # 3 p. 481 - 499
反应条件
in methanol N2 atmosphere; addn. of soln of org. compd. in MeOH to soln. of Au-compd. in MeOH (0°C), stirring (20 h); pptn. on addn. of H2O, filtration, washing (MeOH), drying (vac.);
参考文献
Schmidbaur, Hubert; Brachthaeuser, Benno; Steigelmann, Oliver; Beruda, Holger
Chemische Berichte, 1992 , vol. 125, # 12 p. 2705 - 2710
反应条件
1: iodobenzene dichloride / tetrachloromethane / 1 h / 20 °C / |Inert atmosphere; |Schlenk technique 2: phloroglucinol trimethyl ether / 1,2-dichloro-ethane / 22 h / 150 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Tetrahedron, , vol. 69, # 27-28 p. 5751 - 5757
反应条件
in water-d2 under N2; react. of gold complex with DCl in D2O; detected by NMR;
参考文献
Dalton Transactions, , p. 951 - 958
反应条件
Na[B(3,5-(CF3)2C6H3)4] in THF-d8 (tetrahydrofuran-d8) (Ar); addn. of borate deriv. to THF-d8 soln. of platinum compd. and goldcompd.;
参考文献
Journal of the American Chemical Society, , vol. 133, # 23 p. 8914 - 8926
反应条件
in 1,2-dichloro-ethane T=150°C; 1 h; Inert atmosphereSealed tubeSchlenk technique;
参考文献
Organometallics, , vol. 33, # 6 p. 1328 - 1332
反应条件
in 1,2-dichloro-ethane T=150°C; 5 h; Inert atmosphereSealed tubeSchlenk technique;
参考文献
Organometallics, , vol. 33, # 6 p. 1328 - 1332
反应条件
in benzene slight excess of the phosphine; evapd., recrystd. from benzene-hexane, IR, elem. anal.;
参考文献
Gazzetta Chimica Italiana, , vol. 112, p. 539 - 542
