(3,3-二乙氧基丙基)苯合成路线 （共 20 条）
反应条件
[Rh(1,5-cyclooctadienyl)(μ-OCH3)]2; hydrogen; pyridinium p-toluenesulfonate; triphenylphosphine
T=60°C; P=37503 Torr; 24 h; Title compound not separated from byproducts;
参考文献
Fernandez, Elena; Castillon, Sergio
Tetrahedron Letters, 1994 , vol. 35, # 15 p. 2361 - 2364
反应条件
sodium nitrate
T=30°C; P=760.051 Torr; 4 h;
参考文献
Ge, Changhua; Li, Yan; Zhao, Jie; Zhou, Renxian
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2010 , vol. 49, # 3 p. 281 - 287
反应条件
1: 80 percent / disodium hydrogenphosphate, 6 percent sodium amalgam, methanol / -20 deg C then to RT, 2 h
2: 95 percent / p-toluenesulfonic acid / 2 h
View Scheme
参考文献
Padwa, Albert; Bullock, William H.; Dyszlewski, Andrew D.; McCombie, S. W.; Shankar, B. B.; Ganguly, A. K.
Journal of Organic Chemistry, 1991 , vol. 56, # 11 p. 3556 - 3564
反应条件
ethanol; platinum
Hydrogenation;
参考文献
Sigmund
Monatshefte fuer Chemie, 1929 , vol. 53/54, p. 615
反应条件
diethyl ether; phenyllithium
参考文献
Jones; Law
Journal of the Chemical Society, 1958 , p. 3631
参考文献
Mantione,R. et al.
Bulletin de la Societe Chimique de France, 1967 , p. 2912 - 2918
反应条件
1: (i) EtMgBr, (ii) /BRN= 605384/
View Scheme
参考文献
Mantione,R. et al.
Bulletin de la Societe Chimique de France, 1967 , p. 2912 - 2918
反应条件
1: (i) EtMgBr, (ii) /BRN= 605384/
View Scheme
参考文献
Mantione,R. et al.
Bulletin de la Societe Chimique de France, 1967 , p. 2912 - 2918
参考文献
Sigmund; Marchart
Monatshefte fuer Chemie, 1929 , vol. 53/54, p. 615
反应条件
1: 86 percent / HClO4-SiO2 / H2O; ethanol / 0.25 h / 25 - 30 °C
2: 85 percent / HClO4-SiO2 / 0.03 h / 25 - 30 °C
View Scheme
参考文献
Kumar, Raj; Kumar, Dinesh; Chakraborti, Asit K.
Synthesis, 2007 , # 2 p. 299 - 303
