2-(P-甲氧苄基)氨基嘧啶合成路线 (共 15 条)
反应条件
sodium amide; toluene
参考文献
Mossini; Maggiali; Morini; Impicciatore; Molina
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 3 p. 189 - 199
参考文献
Sunagawa et al.
Yakugaku Zasshi, 1952 , vol. 72, p. 1570,1572
Chem.Abstr., 1953 , p. 9285
反应条件
triethylamine in ethanol
T=120°C; 0.0833333 h; microwave irradiation;
参考文献
Ermolat'ev; Alifanov; Rybakov; Babaev; Van Der Eycken
Synthesis, 2008 , # 13 p. 2083 - 2088
反应条件
hydrogen; palladium on activated charcoal in ethanol; water
T=25 - 30°C; P=5884.07 Torr; 12 h;
参考文献
Mossini; Maggiali; Morini; Impicciatore; Molina
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 3 p. 189 - 199
反应条件
[RuCl(CO)(PPh3)(PNS-Me)]; potassium hydroxide in toluene
T=100°C; 12 h;
参考文献
Ramachandran, Rangasamy; Prakash, Govindan; Selvamurugan, Sellappan; Viswanathamurthi, Periasamy; Malecki, Jan Grzegorz; Ramkumar, Venkatachalam
Dalton Transactions, 2014 , vol. 43, # 21 p. 7889 - 7902
反应条件
potassium fluoride in water
T=100°C; 17 h; Green chemistry;
参考文献
Walsh, Katie; Sneddon, Helen F.; Moody, Christopher J.
ChemSusChem, 2013 , vol. 6, # 8 p. 1455 - 1460
参考文献
Pyridium Corp.
Patent: US2500283 , 1946 ;
Full Text Show Details
Nepera Chem.Co.
Patent: DE829893 , 1951 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Kaye; Kogon
Recueil des Travaux Chimiques des Pays-Bas, 1952 , vol. 71, p. 309,314
Show Details
Lincoln et al.
Journal of the American Chemical Society, 1949 , vol. 71, p. 2902,2903
反应条件
1: ethanol / 3 h / Ambient temperature
2: hydrogen / 10percent Pd/C / ethanol; H2O / 12 h / 25 - 30 °C / 5884.07 Torr
View Scheme
参考文献
Mossini; Maggiali; Morini; Impicciatore; Molina
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 3 p. 189 - 199
反应条件
1: 40 percent / glacial acetic acid / ethanol; benzene / 24 h / Heating
2: 37 percent / NaBH4 / ethanol / 4 h / Heating
View Scheme
参考文献
Fioravanti; Biava; Donnarumma; Porretta; Simonetti; Villa; Porta-Puglia; Deidda; Maullu; Pompei
Farmaco, 1996 , vol. 51, # 10 p. 643 - 652
反应条件
sodium amide; toluene
参考文献
Matsukawa et al.
Yakugaku Zasshi, 1951 , vol. 71, p. 895
Chem.Abstr., 1952 , p. 8122