5,6-二氢-5-甲基尿嘧啶合成路线 （共 30 条）
反应条件
water Irradiationvar. irradiation: γ-radiolysis; Quantum yield;
参考文献
Canadian Journal of Chemistry, , vol. 64, p. 2297 - 2300
参考文献
Monatshefte fuer Chemie, , vol. 17, p. 182
反应条件
in water T=40 - 50°C; 0.666667 h; Irradiationirradiation by argon arch plasma; by hydrogen-oxygen flame; Rate constant;
参考文献
Naraoka, Hiroshi; Takasaki, Michiaki; Nomoto, Shinya; Harada, Kaoru
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 414 - 416
反应条件
oxygen; Nitrous oxide in water P=760 Torr; IrradiationpH=6; also without N2O; with <14C-2> labelled compounds; G-values of degradation products; Product distributionRate constantQuantum yield;
参考文献
Cadet, J.
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1980 , vol. 35, # 12 p. 1579 - 1583
反应条件
oxygen; Nitrous oxide in water IrradiationpH dependence of the yield of products in the radiolysis; Product distribution;
参考文献
Al-Sheikhly, Mohamed I.; Hissung, Alfred; Schuchmann, Heinz-Peter; Schuchmann, Man Nien; Sonntag, Clemens von; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 4 p. 601 - 608
反应条件
oxygen; Nitrous oxide in water IrradiationpH dependence of the yield of products in the radiolysis; Product distribution;
参考文献
Al-Sheikhly, Mohamed I.; Hissung, Alfred; Schuchmann, Heinz-Peter; Schuchmann, Man Nien; Sonntag, Clemens von; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 4 p. 601 - 608
反应条件
1: 63 percent / NaH / dimethylformamide / 8 h / Ambient temperature 2: 1.) LDA / 1.) THF, -78 deg C, 30 min, 2.) THF, -78 deg C, 2 h 3: PBr3 / tetrahydrofuran / 0.17 h / Ambient temperature 4: Bu3SnH, AlBN / toluene / 0.5 h / Heating 5: 40 percent / CAN / acetonitrile; H2O / 2 h / Ambient temperature 6: 70 percent / TFA / 2 h / 60 °C View Scheme
参考文献
Nicewonger, Robb; Begley, Tadhg P.
Tetrahedron Letters, 1997 , vol. 38, # 6 p. 935 - 936
参考文献
Blagoeva,I.B. et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1979 , p. 1115 - 1122
反应条件
hydrogenchloride T=120°C; Kochen der entstandenen Carbonsaeure mit aethanol.HCl;
参考文献
Clemo; Melrose
Journal of the Chemical Society, 1942 , p. 425
反应条件
phosphoric acid; dihydropyrimidinase; N-carbamoyl- -alanine amidohydrolase; nickel dichloride in aq. phosphate buffer T=30°C; pH=8; Enzymatic reaction;
参考文献
Martinez-Gomez, Ana Isabel; Clemente-Jimenez, Josefa Maria; Rodriguez-Vico, Felipe; Kanerva, Liisa T.; Li, Xiang-Guo; Heras-Vazquez, Francisco Javier Las; Martinez-Rodriguez, Sergio
Process Biochemistry, 2012 , vol. 47, # 12 p. 2090 - 2096
