2,5-二甲氧基四氢呋喃合成路线 (共 286 条)
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol T=10 - 20°C; 1.5 h; Yield given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79
参考文献
Liu, Wei; Ma, Yuan; Yin, Yingwu; Zhao, Yufen
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 4 p. 577 - 579
反应条件
4-chloro pyridine hydrochloride in 1,4-dioxane 1 h; Heating;
参考文献
Heterocycles, , vol. 36, # 11 p. 2513 - 2522
反应条件
trifluorormethanesulfonic acid in dichloromethane T=20°C; 2 h;
参考文献
Abid, Mohammed; Teixeira, Liliana; Toeroek, Bela
Tetrahedron Letters, 2007 , vol. 48, # 23 p. 4047 - 4050
反应条件
trifluorormethanesulfonic acid in dichloromethane T=20°C; 2 h;
参考文献
Abid, Mohammed; Teixeira, Liliana; Toeroek, Bela
Tetrahedron Letters, 2007 , vol. 48, # 23 p. 4047 - 4050
反应条件
trifluorormethanesulfonic acid in dichloromethane T=20°C; 2 h; Title compound not separated from byproducts.;
参考文献
Abid, Mohammed; Teixeira, Liliana; Toeroek, Bela
Tetrahedron Letters, 2007 , vol. 48, # 23 p. 4047 - 4050
反应条件
trifluorormethanesulfonic acid in dichloromethane T=20°C; 2 h; Title compound not separated from byproducts.;
参考文献
Abid, Mohammed; Teixeira, Liliana; Toeroek, Bela
Tetrahedron Letters, 2007 , vol. 48, # 23 p. 4047 - 4050
反应条件
acetic acid T=120°C; 1 h;
参考文献
Steiner; Gries; Lenke
Journal of Medicinal Chemistry, 1981 , vol. 24, # 1 p. 59 - 63
反应条件
tungstophosphoric acid supported on silica gel 20 h; Microwave irradiationNeat (no solvent);
参考文献
Mahmoudi, Hajar; Jafari, Abbas Ali
ChemCatChem, 2013 , vol. 5, # 12 p. 3743 - 3749
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol T=10 - 20°C; 1.5 h; Yield given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79