2,5-二甲氧基四氢呋喃合成路线 (共 286 条)
反应条件
hydrogenchloride in ethanol
0.5 h; Heating;
参考文献
Stefancich; Artico; Corelli; Massa
Synthesis, 1983 , vol. No. 9, p. 757 - 759
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol
T=10 - 20°C; 1.5 h; Yield given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79
反应条件
toluene-4-sulfonic acid in toluene
1 h; Reflux;
参考文献
Faigl, Ferenc; Matravoelgyi, Bela; Deak, Szilvia; Holczbauer, Tamas; Czugler, Matyas; Balazs, Laszlo; Hermecz, Istvan
Tetrahedron, 2012 , vol. 68, # 22 p. 4259 - 4266
反应条件
in acetic acid
2 h; Heating;
参考文献
Balli, Heinz; Zeller, Martin
Helvetica Chimica Acta, 1983 , vol. 66, # 7 p. 2135 - 2139
反应条件
4-chloro pyridine hydrochloride in 1,4-dioxane
Clauson-Kaas conditions; 24 h; Reflux;
参考文献
Aiello, Francesca; Garofalo, Antonio; Grande, Fedora
Tetrahedron Letters, 2011 , vol. 52, # 44 p. 5824 - 5826
反应条件
hydrogenchloride; acetic acid in 1,4-dioxane; water
T=20°C; Clauson-Kaas reaction; 24 h; Reflux;
参考文献
Lellouche, Jean-Paul; Pomerantz, Zvika; Ghosh, Subrata
Tetrahedron Letters, 2011 , vol. 52, # 51 p. 6903 - 6907
反应条件
in N,N-dimethyl-formamide
T=150 - 160°C; 0.0833333 h;
参考文献
Artico, Marino; Corelli, Federico; Massa, Silvio; Stefancich, Giorgio
Synthesis, 1983 , # 11 p. 931
反应条件
in N,N-dimethyl-formamide
T=150 - 160°C; 0.0833333 h;
参考文献
Artico, Marino; Corelli, Federico; Massa, Silvio; Stefancich, Giorgio
Synthesis, 1983 , # 11 p. 931
反应条件
T=180°C; 0.666667 h;
参考文献
Uno, Toshio; Takamatsu, Masanori; Inoue, Yoshimasa; Kawahata, Yoshihiro; Iuchi, Koji; Tsukamoto, Goro
Journal of Medicinal Chemistry, 1987 , vol. 30, # 12 p. 2163 - 2169
参考文献
Faigl, Ferenc; Vas-Feldhoffer, Bernadett; Kubinyi, Miklos; Pal, Krisztina; Tarkanyi, Gabor; Czugler, Matyas
Tetrahedron Asymmetry, 2009 , vol. 20, # 1 p. 98 - 103