2,5-二甲氧基四氢呋喃合成路线 (共 286 条)
反应条件
sodium acetate; acetic acid
0.5 h; Heating;
参考文献
Sircar; Winters; Quin III; Lu; Major; Panek
Journal of Medicinal Chemistry, 1993 , vol. 36, # 12 p. 1735 - 1745
反应条件
sodium acetate; acetic acid
参考文献
Shmatova, Olga I.; Shevchenko, Nikolay E.; Balenkova, Elizabeth S.; Roeschenthaler, Gerd-Volker; Nenajdenko, Valentine G.
Mendeleev Communications, 2013 , vol. 23, # 2 p. 92 - 93
反应条件
acetic acid
Clauson-Kaas reaction; 0.25 h; Heating;
参考文献
Sheremetev; Konkina; Yudin; Dmitriev; Averkiev; Antipin
Russian Chemical Bulletin, 2003 , vol. 52, # 7 p. 1413 - 1418
反应条件
acetic acid
T=110 - 120°C; 3 h; Heating / reflux;
参考文献
RANBAXY LABORATORIES LIMITED
Patent: WO2006/38100 A1, 2006 ;
Location in patent: Page/Page column 77 ;
反应条件
acetic acid
Clauson-Kaas Synthesis; 0.5 h; Reflux;
参考文献
Conte, Sean; Rodriguez-Calero, Gabriel G.; Burkhardt, Stephen E.; Lowe, Michael A.; Abruna, Hector D.
RSC Advances, 2013 , vol. 3, # 6 p. 1957 - 1964
反应条件
potassium acetate; acetic acid
4.25 h; Heating;
参考文献
Larsen; Connell; Cudahy; Evans; May; Meglasson; O'Sullivan; Schostarez; Sih; Stevens; Tanis; Tegley; Tucker; Vaillancourt; Vidmar; Watt; Yu
Journal of Medicinal Chemistry, 2001 , vol. 44, # 8 p. 1217 - 1230
反应条件
acetic acid
Condensation; aromatization; 2 h; Heating;
参考文献
Lee, Chang Kiu; Jun, Jung Ho; Yu, Ji Sook
Journal of Heterocyclic Chemistry, 2000 , vol. 37, # 1 p. 15 - 24
反应条件
trifluorormethanesulfonic acid in dichloromethane
T=0 - 20°C; 2 h; Inert atmosphere;
参考文献
Rafiq, Settu Muhamad; Sivasakthikumaran, Ramakrishnan; Mohanakrishnan, Arasambattu K.
Organic Letters, 2014 , vol. 16, # 10 p. 2720 - 2723
反应条件
montmorillonite K-10
T=100°C; 0.05 h; microwave irradiation;
参考文献
Abid, Mohammed; Landge, Shainaz M.; Toeroek, Bela
Organic Preparations and Procedures International, 2006 , vol. 38, # 5 p. 495 - 500
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol
T=10 - 20°C; 1.5 h; Yield given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79