2,5-二甲氧基四氢呋喃合成路线 （共 286 条）
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol
T=10 - 20°C; 1.5 h; Yield given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79
反应条件
trifluorormethanesulfonic acid in dichloromethane
T=0 - 20°C; 2 h; Inert atmosphere; Reagent/catalyst;
参考文献
Rafiq, Settu Muhamad; Sivasakthikumaran, Ramakrishnan; Mohanakrishnan, Arasambattu K.
Organic Letters, 2014 , vol. 16, # 10 p. 2720 - 2723
反应条件
montmorillonite K-10
T=100°C; 0.05 h; microwave irradiation;
参考文献
Abid, Mohammed; Landge, Shainaz M.; Toeroek, Bela
Organic Preparations and Procedures International, 2006 , vol. 38, # 5 p. 495 - 500
反应条件
trifluorormethanesulfonic acid in dichloromethane
T=0 - 20°C; 2 h; Inert atmosphere;
参考文献
Rafiq, Settu Muhamad; Sivasakthikumaran, Ramakrishnan; Mohanakrishnan, Arasambattu K.
Organic Letters, 2014 , vol. 16, # 10 p. 2720 - 2723
反应条件
water
T=140°C; Paal-Knorr pyrrole synthesis; 0.333333 h; Microwave irradiation;
参考文献
Polshettiwar, Vivek; Varma, Rajender S.
Tetrahedron, 2010 , vol. 66, # 5 p. 1091 - 1097
反应条件
Bi(NO3)3·5H2O in tetrahydrofuran
T=110°C; 0.5 h; Microwave irradiation;
参考文献
Rivera, Sonya; Bandyopadhyay, Debasish; Banik, Bimal K.
Tetrahedron Letters, 2009 , vol. 50, # 39 p. 5445 - 5448
反应条件
sodium acetate; acetic acid
T=80°C;
参考文献
Settambolo, Roberta; Guazzelli, Giuditta; Mengali, Lucia; Mandoli, Alessandro; Lazzaroni, Raffaello
Tetrahedron Asymmetry, 2003 , vol. 14, # 17 p. 2491 - 2493
反应条件
acetic acid in water; 1,2-dichloro-ethane
3 h; Heating;
参考文献
Demir, Ayhan S.; Subasi, N. Tuna; Sahin, Ertan
Tetrahedron Asymmetry, 2006 , vol. 17, # 18 p. 2625 - 2631
反应条件
phosphorus pentoxide in toluene
T=110°C; 0.166667 h;
参考文献
Fang; Leysen; Ottenheijm
Synthetic Communications, 1995 , vol. 25, # 12 p. 1857 - 1861
反应条件
sodium acetate in acetic acid
T=80°C; 0.5 h;
参考文献
Kashima, Choji; Maruyama, Tatsuya; Harada, Kazuo; Hibi, Shigeki; Omote, Yoshimori
Journal of Chemical Research, Miniprint, 1988 , # 2 p. 601 - 645
