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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘苯甲醚
合成路线
（共 1687 条）
696-62-8
4-碘苯甲醚
→
反应条件
27088-84-2
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=85°C; Stille coupling; 3 h;
参考文献
Vachal, Petr; Toth, Leslie M.
Tetrahedron Letters, 2004 , vol. 45, # 38 p. 7157 - 7161
696-62-8
4-碘苯甲醚
+
178215-64-0
→
反应条件
2584-37-4
1-甲基-4-苯基-1H-喹啉-2-酮
反应条件
tris(4-methylphenyl)-phosphine; silver carbonate; palladium (II) bromide in N,N-dimethyl acetamide; toluene T=150°C; 1 h; Sealed tubeInert atmosphereMicrowave irradiationSchlenk technique;
参考文献
Carrer, Amandine; Brion, Jean-Daniel; Messaoudi, Samir; Alami, Mouad
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 10 p. 2044 - 2054
696-62-8
4-碘苯甲醚
+
178215-64-0
→
反应条件
1033342-93-6
+
2584-37-4
1-甲基-4-苯基-1H-喹啉-2-酮
反应条件
silver(I) acetate; triphenylphosphine; palladium (II) bromide in N,N-dimethyl acetamide; toluene T=150°C; 1 h; Sealed tubeInert atmosphereMicrowave irradiationSchlenk technique;
参考文献
Carrer, Amandine; Brion, Jean-Daniel; Messaoudi, Samir; Alami, Mouad
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 10 p. 2044 - 2054
696-62-8
4-碘苯甲醚
+
100-66-3
苯甲醚
→
反应条件
53040-92-9
4-甲氧基-4-甲基-联苯
+
24423-07-2
(7CI,8CI)-m-(对甲苯)-苯甲醚
+
92495-53-9
反应条件
iron(III) triphenantroline chloride; potassium tert-butylate T=100°C; 24 h; Inert atmosphere; Overall yield = 65 percent; Overall yield = 64 mg;
参考文献
Huang, Yuxing; Moret, Marc-Etienne; Klein Gebbink, Robertus J. M.
European Journal of Organic Chemistry, 2014 , vol. 2014, # 18 p. 3788 - 3793
624-31-7
4-碘甲苯
+
696-62-8
4-碘苯甲醚
+
1066-54-2
三甲基乙炔基硅
→
反应条件
24785-38-4
反应条件
1: para-iodoanisole; trimethylsilylacetylene With potassium carbonate in methanol; acetonitrile T=40°C; Sonogashira Cross-Coupling; 2 h; 2: 1-(iodo)-4-methylbenzene in methanol; acetonitrile T=40°C; Sonogashira Cross-Coupling; 2 h; chemoselective reaction;
参考文献
Mandali, Pavan Kumar; Chand, Dillip Kumar
Catalysis Communications, 2014 , vol. 47, p. 40 - 44
696-62-8
4-碘苯甲醚
+
766-97-2
4-甲苯基乙炔
→
反应条件
24785-38-4
反应条件
Cu(acac)2*H2O; potassium carbonate; dimethyl sulfoxide T=140°C; Sonogashira coupling; 24 h; Inert atmosphere;
参考文献
Li, Tingyi; Qu, Xiaoming; Xie, Guanlei; Mao, Jincheng
Chemistry - An Asian Journal, 2011 , vol. 6, # 6 p. 1325 - 1330
696-62-8
4-碘苯甲醚
+
2227-58-9
→
反应条件
24785-38-4
反应条件
copper(l) iodide; potassium carbonate; triphenylphosphine in dimethyl sulfoxide T=90°C; 24 h; Inert atmosphere;
参考文献
Qu, Xiaoming; Li, Tingyi; Sun, Peng; Zhu, Yan; Yang, Hailong; Mao, Jincheng
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 6938 - 6942
60512-56-3
1-(2,2-二溴乙烯)-4-甲基苯
+
696-62-8
4-碘苯甲醚
→
反应条件
24785-38-4
反应条件
aluminum oxide; potassium fluoride; copper(l) iodide; triphenylphosphine; nickel 0.05 h; microwave irradiation;
参考文献
Yan, Jincan; Wang, Zhiyuan; Wang, Lei
Journal of Chemical Research, 2004 , # 1 p. 71 - 73
696-62-8
4-碘苯甲醚
→
反应条件
24785-38-4
反应条件
1: para-iodoanisole With n-butyllithium in diethyl ether; hexane Inert atmosphereCooling; 2: 1-(4'-methylphenylsulfonyl)-2-(4'-methylphenyl)ethyne in diethyl ether; hexane 0.25 h; Inert atmosphere; regioselective reaction;
参考文献
Garcia Ruano, Jose Luis; Aleman, Jose; Marzo, Leyre; Alvarado, Cuauhtemoc; Tortosa, Mariola; Diaz-Tendero, Sergio; Fraile, Alberto
Chemistry - A European Journal, 2012 , vol. 18, # 27 p. 8414 - 8422
696-62-8
4-碘苯甲醚
→
反应条件
16473-39-5
反应条件
1: copper(l) iodide; sodium carbonate / dimethyl sulfoxide / 20 h / 80 °C 2: tri-n-butyl-tin hydride; 2,2'-azo-bisisobutyronitrile / toluene / 8 h / 110 °C View Scheme
参考文献
Zhao, Yanchuan; Ni, Chuanfa; Jiang, Fanzhou; Gao, Bing; Shen, Xiao; Hu, Jinbo
ACS Catalysis, 2013 , vol. 3, # 4 p. 631 - 634
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