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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘苯甲醚
合成路线
（共 1687 条）
696-62-8
4-碘苯甲醚
→
反应条件
922495-42-9
反应条件
1.1: 1,10-phenanthroline; copper(l) chloride; potassium hydroxide / anhydrous xylene / 72 h / 140 °C / Inert atmosphere 2.1: trichlorophosphate / 48 h / 0 - 120 °C / Inert atmosphere 2.2: 20 °C / Inert atmosphere; Cooling with ice 3.1: pyridine; hydroxylamine hydrochloride; acetic acid / N,N-dimethyl-formamide / 9 h / 130 °C / Inert atmosphere 4.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 90 h / Inert atmosphere; Reflux View Scheme
参考文献
He, Ze; Kan, Chi-Wai; Ho, Cheuk-Lam; Wong, Wai-Yeung; Chui, Chung-Hin; Tong, Ka-Lap; So, Shu-Kong; Lee, Tik-Ho; Leung, Louis M.; Lin, Zhenyang
Dyes and Pigments, 2011 , vol. 88, # 3 p. 333 - 343
696-62-8
4-碘苯甲醚
+
100-66-3
苯甲醚
→
反应条件
53040-92-9
4-甲氧基-4-甲基-联苯
+
24423-07-2
(7CI,8CI)-m-(对甲苯)-苯甲醚
+
92495-53-9
反应条件
iron(III) triphenantroline chloride; potassium tert-butylate T=100°C; 24 h; Inert atmosphere; Overall yield = 65 percent; Overall yield = 64 mg;
参考文献
Huang, Yuxing; Moret, Marc-Etienne; Klein Gebbink, Robertus J. M.
European Journal of Organic Chemistry, 2014 , vol. 2014, # 18 p. 3788 - 3793
696-62-8
4-碘苯甲醚
+
16419-60-6
2-甲基苯硼酸
→
反应条件
92495-54-0
4-甲氧基-2-甲基-联苯
反应条件
potassium carbonate; [PS-PEG-adppp-Pd(η3-C3H5)]Cl in water T=50°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Ye, Yue-Mei; Wang, Bin-Bin; Ma, Dan; Shao, Li-Xiong; Lu, Jian-Mei
Catalysis Letters, 2010 , vol. 139, # 3-4 p. 141 - 144
696-62-8
4-碘苯甲醚
+
80137-71-9
→
反应条件
92495-54-0
4-甲氧基-2-甲基-联苯
反应条件
potassium carbonate; palladium diacetate in water; acetone T=65°C; 0.666667 h;
参考文献
Wallow, Thomas I.; Novak, Bruce M.
Journal of Organic Chemistry, 1994 , vol. 59, # 17 p. 5034 - 5037
696-62-8
4-碘苯甲醚
+
188404-95-7
→
反应条件
92495-54-0
4-甲氧基-2-甲基-联苯
反应条件
tetrakis(triphenylphosphine) palladium(0); silver(l) oxide in tetrahydrofuran T=60°C; Arylation; 36 h;
参考文献
Hirabayashi, Kazunori; Kawashima, Jun; Nishihara, Yasushi; Mori, Atsunori; Hiyama, Tamejiro
Organic Letters, 1999 , vol. 1, # 2 p. 299 - 301
696-62-8
4-碘苯甲醚
+
84109-17-1
→
反应条件
92495-54-0
4-甲氧基-2-甲基-联苯
反应条件
tetrabutylammomium bromide; palladium diacetate in tetrahydrofuran T=20°C; Negishi coupling; 4 h; Inert atmosphere;
参考文献
Liu, Jing; Deng, Yi; Wang, Haibo; Zhang, Hua; Yu, Ganxiang; Wu, Bingbin; Zhang, Heng; Li, Qiang; Marder, Todd B.; Yang, Zhen; Lei, Aiwen
Organic Letters, 2008 , vol. 10, # 13 p. 2661 - 2664
696-62-8
4-碘苯甲醚
+
108-88-3
甲苯
→
反应条件
53040-92-9
4-甲氧基-4-甲基-联苯
+
17171-17-4
4-甲氧基-3-甲基联苯
+
92495-54-0
4-甲氧基-2-甲基-联苯
反应条件
bathophenanthroline; potassium tert-butylate; ferrous acetate T=20 - 80°C; Inert atmosphere;
参考文献
Qiu, Yatao; Liu, Yanghan; Yang, Kai; Hong, Wenkun; Li, Zheng; Wang, Zhaoyang; Yao, Zhiyi; Jiang, Sheng
Organic Letters, 2011 , vol. 13, # 14 p. 3556 - 3559
615-37-2
+
696-62-8
4-碘苯甲醚
→
反应条件
92495-54-0
4-甲氧基-2-甲基-联苯
反应条件
1: para-iodoanisole With [PdCl2(1,3-bis(diphenylphosphino)propane)]; tBuCH2CH2B(H)NiPr2; triethylamine; potassium iodide in toluene T=110°C; Suzuki coupling; 1 h; Inert atmosphere; 2: 1-iodo-2-methylbenzene With caesium carbonate in ethanol; water; toluene T=90°C; Suzuki coupling; 15 h; Inert atmosphere;
参考文献
Marciasini, Ludovic; Richy, Nicolas; Vaultier, Michel; Pucheault, Mathieu
Chemical Communications, 2012 , vol. 48, # 10 p. 1553 - 1555
696-62-8
4-碘苯甲醚
+
10050-08-5
→
反应条件
92495-54-0
4-甲氧基-2-甲基-联苯
反应条件
2,2'-biquinoline; 10 Pd/C; cesium fluoride in 1-methyl-pyrrolidin-2-one T=140°C; 24 h; Inert atmosphere;
参考文献
Monguchi, Yasunari; Hattori, Tomohiro; Miyamoto, Yasuhiro; Yanase, Takayoshi; Sawama, Yoshinari; Sajiki, Hironao
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2561 - 2567
696-62-8
4-碘苯甲醚
+
7029-31-4
→
反应条件
92495-54-0
4-甲氧基-2-甲基-联苯
反应条件
in tetrahydrofuran T=110°C; Inert atmosphere;
参考文献
Minami, Hiroki; Wang, Xuan; Wang, Chao; Uchiyama, Masanobu
European Journal of Organic Chemistry, 2013 , # 35 p. 7891 - 7894
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