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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘苯甲醚
合成路线
（共 1687 条）
696-62-8
4-碘苯甲醚
+
108-98-5
硫酚
→
反应条件
5335-87-5
4,4'-二甲氧基二苯二硫
+
5633-57-8
1-甲氧基-4-(苯硫基)-苯
反应条件
potassium carbonate in acetonitrile T=100°C; 0.5 h; Microwave irradiation;
参考文献
Gonzalez-Arellano, Camino; Luque, Rafael; MacQuarrie, Duncan J.
Chemical Communications, 2009 , # 11 p. 1410 - 1412
696-62-8
4-碘苯甲醚
→
反应条件
5335-87-5
4,4'-二甲氧基二苯二硫
+
3393-77-9
4,4’-二甲氧基二苯硫醚
反应条件
sulfur; copper(l) iodide; lithium hydroxide hydrate in N,N-dimethyl-formamide T=100°C; 168 h; Inert atmosphere;
参考文献
Organometallics, , vol. 32, # 19 p. 5514 - 5522
4885-02-3
二氯甲基甲醚
+
696-62-8
4-碘苯甲醚
→
反应条件
42298-41-9
2-甲氧基-5-碘苯甲醛
反应条件
1: para-iodoanisole With titanium tetrachloride in dichloromethane T=0°C; 0.5 h; 2: dichloromethoxy methane in dichloromethane T=0°C; 2 h;
参考文献
Pfizer Inc.
Patent: US6369074 B1, 2002 ;
Location in patent: Page column 27 ;
US 6369074 B1
696-62-8
4-碘苯甲醚
→
反应条件
3672-48-8
5-(4-甲氧基苯基)异噁唑
反应条件
1: [Pd(η3-1-Ph-allyl)(μ-Cl)]2; N,N-dicyclohexylmethylamine; N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 / 1,4-dioxane / 17 h / 100 °C / Inert atmosphere 2: hydrogenchloride; hydroxylamine hydrochloride / ethanol; water / 16 h / 80 °C / Inert atmosphere View Scheme
参考文献
Gogsig, Thomas M.; Nielsen, Dennis U.; Lindhardt, Anders T.; Skrydstrup, Troels
Organic Letters, 2012 , vol. 14, # 10 p. 2536 - 2539
696-62-8
4-碘苯甲醚
+
20277-69-4
甲烷亚磺酸钠
→
反应条件
3517-90-6
4-甲氧基苯甲砜
反应条件
copper(l) iodide in dimethyl sulfoxide 24 h; Heating;
参考文献
Shen, Chao; Xu, Jun; Yu, Wenbo; Zhang, Pengfei
Green Chemistry, 2014 , vol. 16, # 6 p. 3007 - 3012
696-62-8
4-碘苯甲醚
+
74-88-4
→
反应条件
3517-90-6
4-甲氧基苯甲砜
反应条件
1: para-iodoanisole With 1,10-phenanthroline; K2S2O5; tetrabutylammomium bromide; sodium formate; palladium diacetate; triphenylphosphine in dimethyl sulfoxide T=70°C; 2 h; Inert atmosphereMicrowave irradiation; 2: methyl iodide in dimethyl sulfoxide T=23°C; 20 h; Inert atmosphere; Reagent/catalystSolvent; chemoselective reaction;
参考文献
Shavnya, Andrei; Coffey, Steven B.; Smith, Aaron C.; Mascitti, Vincent
Organic Letters, 2013 , vol. 15, # 24 p. 6226 - 6229
696-62-8
4-碘苯甲醚
+
19186-23-3
→
反应条件
3517-90-6
4-甲氧基苯甲砜
反应条件
(CuOTf)2.C6H6; sodium carbonate; N-methyl-2-(methylamino)ethylamine in dimethyl sulfoxide T=110°C; 20 h;
参考文献
Coelho Jr., Richard V.; Schildknegt, Klaas
Journal of Labelled Compounds and Radiopharmaceuticals, 2010 , vol. 53, # 5-6 p. 427 - 429
696-62-8
4-碘苯甲醚
→
反应条件
3517-90-6
4-甲氧基苯甲砜
反应条件
1: K2S2O5; tetrabutylammomium bromide; sodium formate; palladium diacetate; triphenylphosphine; 1,10-phenanthroline / acetonitrile / 2 h / 70 °C / |Inert atmosphere; |Microwave irradiation 2: dimethyl sulfoxide / 20 h / 23 °C / |Inert atmosphere View Scheme
参考文献
Shavnya, Andrei; Coffey, Steven B.; Smith, Aaron C.; Mascitti, Vincent
Organic Letters, 2013 , vol. 15, # 24 p. 6226 - 6229
696-62-8
4-碘苯甲醚
+
67-68-5
→
反应条件
3517-90-6
4-甲氧基苯甲砜
反应条件
copper(I) oxide; potassium tert-butylate; oxygen; acetylacetone T=100°C; 20 h;
参考文献
Yuan, Gaoqing; Zheng, Junhua; Gao, Xiaofang; Li, Xianwei; Huang, Liangbin; Chen, Huoji; Jiang, Huanfeng
Chemical Communications, 2012 , vol. 48, # 60 p. 7513 - 7515
5798-75-4
+
696-62-8
4-碘苯甲醚
→
反应条件
47230-38-6
+
732-80-9
反应条件
manganese; cobalt (II) bromide; triphenylphosphine; trifluoroacetic acid in pyridine; N,N-dimethyl-formamide T=50°C;
参考文献
Amatore, Muriel; Gosmini, Corinne
Angewandte Chemie - International Edition, 2008 , vol. 47, # 11 p. 2089 - 2092
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