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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘苯甲醚
合成路线
（共 1687 条）
696-62-8
4-碘苯甲醚
+
25015-63-8
频哪醇硼烷
→
反应条件
100-66-3
苯甲醚
+
171364-79-7
4-甲氧基苯硼酸频那醇酯
反应条件
triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; borylation; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 65, # 1 p. 164 - 168
696-62-8
4-碘苯甲醚
+
73183-34-3
联硼酸频那醇酯
→
反应条件
2132-80-1
4,4-二甲氧基联苯
+
171364-79-7
4-甲氧基苯硼酸频那醇酯
反应条件
potassium acetate; palladium diacetate in N,N-dimethyl-formamide T=80°C; 2 h;
参考文献
Zhu, Lei; Duquette, Jason; Zhang, Mingbao
Journal of Organic Chemistry, 2003 , vol. 68, # 9 p. 3729 - 3732
696-62-8
4-碘苯甲醚
+
185990-03-8
2-(二甲基苯甲硅烷)-4,4,5,5-四甲基-1,3,2-二氧环戊硼烷
→
反应条件
171364-79-7
4-甲氧基苯硼酸频那醇酯
反应条件
1: Me2PhSiBpin With potassium methanolate in ethylene glycol dimethyl ether T=30°C; 0.166667 h; Inert atmosphere; 2: para-iodoanisole in ethylene glycol dimethyl ether T=30°C; 1 h;
参考文献
Yamamoto, Eiji; Izumi, Kiyotaka; Horita, Yuko; Ito, Hajime
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19997 - 20000
696-62-8
4-碘苯甲醚
→
反应条件
171364-79-7
4-甲氧基苯硼酸频那醇酯
反应条件
1: triethylamine; 1,1'-bis(di-tert-butylphosphino)ferrocene palladium dichloride / 1,4-dioxane / 6 h / 80 °C / |Sealed tube 2: hydrogenchloride / water / 15 h / 20 °C View Scheme
参考文献
Murata, Miki; Hirai, Nobuyoshi; Okuyama, Michihiro; Namikoshi, Takeshi; Watanabe, Shinji
Heterocycles, 2014 , vol. 88, # 1 p. 193 - 199
637-69-4
4-甲氧基苯乙烯
+
696-62-8
4-碘苯甲醚
→
反应条件
4705-34-4
4,4'-二甲氧基芪
反应条件
potassium carbonate in N,N-dimethyl-formamide T=110°C; Heck Reaction; 6 h; Inert atmosphere;
参考文献
Sharma, Dharminder; Kumar, Sandeep; Shil, Arun K.; Guha, Nitul Ranjan; Bandna; Das, Pralay
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7044 - 7051
696-62-8
4-碘苯甲醚
+
824985-52-6
→
反应条件
4705-34-4
4,4'-二甲氧基芪
反应条件
tetrabutyl ammonium fluoride; tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran T=65°C; Hiyama cross-coupling; 2 h;
参考文献
Prukala, Wieslaw; Pawluc, Piotr; Posala, Krystian; Marciniec, Bogdan
Synlett, 2008 , # 1 p. 41 - 44
696-62-8
4-碘苯甲醚
+
754-05-2
乙烯基三甲基硅烷
→
反应条件
4705-34-4
4,4'-二甲氧基芪
反应条件
1: With potassium fluoride; tetrabutyl-ammonium chloride; bis(dibenzylideneacetone)-palladium(0) in toluene T=20°C; Heck; 2: With potassium fluoride; tetrabutyl-ammonium chloride; potassium carbonate; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium(0) in water; N,N-dimethyl-formamide; toluene T=85°C; Heck;
参考文献
Jeffery, Tuyet; Ferber, Benoit
Tetrahedron Letters, 2003 , vol. 44, # 1 p. 193 - 197
108-05-4
醋酸乙烯酯
+
696-62-8
4-碘苯甲醚
→
反应条件
4705-34-4
4,4'-二甲氧基芪
反应条件
tributyl-amine; montmorilloniteethylsilyldiphenylphosphinepalladium(II)chloride T=100°C; 24 h;
参考文献
Choudary, B. M.; Sarma, M. Ravichandra
Tetrahedron Letters, 1990 , vol. 31, # 10 p. 1495 - 1496
54509-73-8
+
696-62-8
4-碘苯甲醚
→
反应条件
637-69-4
4-甲氧基苯乙烯
+
4705-34-4
4,4'-二甲氧基芪
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in acetonitrile T=70°C; Mizoroki-Heck reaction; 24 h;
参考文献
Hirabayashi, Kazunori; Ando, Jun-Ichi; Kawashima, Jun; Nishihara, Yasushi; Mori, Atsunori; Hiyama, Tamejiro
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 6 p. 1409 - 1417
696-62-8
4-碘苯甲醚
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
4356-69-8
1,1-二(对茴香基)乙烯
+
4705-34-4
4,4'-二甲氧基芪
反应条件
1: 4-ethynyl-1-methoxy-benzene With benzo[1,3,2]dioxaborole; 1,3-dibutyl-4,5-dichloro-imidazole-1,3-divinylsiloxane Pt(0) in tetrahydrofuran T=25°C; 3 h; 2: para-iodoanisole With potassium carbonate in tetrahydrofuran; 1,4-dioxane T=110°C; Suzuki-Miyaura couplimg reaction; 16 h; Further stages.;
参考文献
Lillo, Vanesa; Mata, Jose A.; Segarra, Anna M.; Peris, Eduardo; Fernandez, Elena
Chemical Communications, 2007 , # 21 p. 2184 - 2186
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