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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘苯甲醚
合成路线
(共 1687 条)
2554-06-5
2,4,6,8-四甲基-2,4,6,8-四乙烯基环四硅氧烷
+
696-62-8
4-碘苯甲醚
→
反应条件
637-69-4
4-甲氧基苯乙烯
+
4705-34-4
4,4'-二甲氧基芪
反应条件
1: D4v With tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 0.166667 h; 2: para-iodoanisole With bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=20°C; Heck reaction; 4 h;
参考文献
Denmark, Scott E.; Wang, Zhigang
Journal of Organometallic Chemistry, 2001 , vol. 624, # 1-2 p. 372 - 375
696-62-8
4-碘苯甲醚
→
反应条件
4705-34-4
4,4'-二甲氧基芪
反应条件
[PdCl2P(OCH2CMe2NH)OCH2CMe2NH2]; tetrabutyl ammonium fluoride in tetrahydrofuran T=60°C; Hiyama coupling; 12 h; Inert atmosphere; diastereoselective reaction;
参考文献
Skarynska, Anna; Majchrzak, Mariusz; Trzeciak, Anna M.; Marciniec, Bogdan
Journal of Molecular Catalysis A: Chemical, 2011 , vol. 351, p. 128 - 135
75-30-9
2-碘代丙烷
+
696-62-8
4-碘苯甲醚
→
反应条件
4132-48-3
反应条件
1: 2-iodo-propane With zinc in tetrahydrofuran T=20°C; Inert atmosphere; 2: para-iodoanisole With terpyridine; nickel dichloride in tetrahydrofuran T=40°C; Negishi coupling reaction; 17 h; Inert atmosphere;
参考文献
Joshi-Pangu, Amruta; Ganesh, Madhu; Biscoe, Mark R.
Organic Letters, 2011 , vol. 13, # 5 p. 1218 - 1221
696-62-8
4-碘苯甲醚
+
77047-87-1
→
反应条件
4132-48-3
+
100-66-3
反应条件
C30H21F6N2NiO2P in tetrahydrofuran T=70°C; 24 h; Schlenk techniqueInert atmosphere; TemperatureConcentration; chemoselective reaction;
参考文献
Weidauer, Maik; Irran, Elisabeth; Someya, Chika I.; Haberberger, Michael; Enthaler, Stephan
Journal of Organometallic Chemistry, 2013 , vol. 729, p. 53 - 59
696-62-8
4-碘苯甲醚
→
反应条件
94608-23-8
反应条件
tetrabutyl ammonium fluoride; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=20 - 25°C; Hiyama coupling; 1 h; Inert atmosphere;
参考文献
Sore, Hannah F.; Blackwell, David T.; MacDonald, Simon J. F.; Spring, David R.
Organic Letters, 2010 , vol. 12, # 12 p. 2806 - 2809
696-62-8
4-碘苯甲醚
+
586-78-7
→
反应条件
92-93-3
反应条件
palladium diacetate; sodium hydroxide; triphenylphosphine; red-coil triblock oligomer derivative T=25°C; Suzuki cross-coupling; 12 h;
参考文献
Lee, Myongsoo; Jang, Cheong-Jin; Ryu, Ja-Hyoung
Journal of the American Chemical Society, 2004 , vol. 126, # 26 p. 8082 - 8083
201230-82-2
+
696-62-8
4-碘苯甲醚
+
107-08-4
→
反应条件
4160-51-4
反应条件
copper; zinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=50°C; P=760 Torr; 22 h;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yamada, Yoshimi; Yoshida, Zen-ichi
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3869 - 3872
102-82-9
+
696-62-8
4-碘苯甲醚
→
反应条件
4160-51-4
反应条件
dichloro bis(acetonitrile) palladium(II); tetrabutylammomium bromide; water; zinc oxide in dimethyl sulfoxide T=100°C; 16 h;
参考文献
Liu, Yan; Yao, Bo; Deng, Chen-Liang; Tang, Ri-Yuan; Zhang, Xing-Guo; Li, Jin-Heng
Organic Letters, 2011 , vol. 13, # 9 p. 2184 - 2187
696-62-8
4-碘苯甲醚
+
123-72-8
→
反应条件
4160-51-4
反应条件
dichloro bis(acetonitrile) palladium(II); tetrabutylammomium bromide; dibutylamine; zinc oxide in dimethyl sulfoxide T=100°C; 16 h;
参考文献
Liu, Yan; Yao, Bo; Deng, Chen-Liang; Tang, Ri-Yuan; Zhang, Xing-Guo; Li, Jin-Heng
Organic Letters, 2011 , vol. 13, # 9 p. 2184 - 2187
696-62-8
4-碘苯甲醚
+
4383-27-1
→
反应条件
4160-51-4
反应条件
dichloro bis(acetonitrile) palladium(II); tetrabutylammomium bromide; water; zinc oxide in dimethyl sulfoxide T=100°C; 48 h;
参考文献
Liu, Yan; Yao, Bo; Deng, Chen-Liang; Tang, Ri-Yuan; Zhang, Xing-Guo; Li, Jin-Heng
Organic Letters, 2011 , vol. 13, # 9 p. 2184 - 2187
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