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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘苯甲醚
合成路线
（共 1687 条）
3240-34-4
碘苯二乙酸
+
696-62-8
4-碘苯甲醚
→
反应条件
183593-98-8
2-乙酰氧基-4-碘-1-甲氧基-苯
+
281191-48-8
反应条件
chloro{1-tert-butyl-3-[(p-tolylsulfinyl)methyl]imidazol-2-ylidene}palladium(II) in acetic anhydride; acetic acid T=95°C; 16 h; Sealed tube; Overall yield = 58percent; Overall yield = 34 mg;
参考文献
Tato, Francisco; Garcia-Dominguez, Andres; Cardenas, Diego J.
Organometallics, 2013 , vol. 32, # 24 p. 7487 - 7494
626-05-1
2,6-二溴吡啶
+
696-62-8
4-碘苯甲醚
→
反应条件
21172-80-5
反应条件
1: 2,6-Dibromopyridine With nBu4ZnLi2*TMEDA in toluene T=20°C; 1.5 h; Inert atmosphere; 2: para-iodoanisole With bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine in toluene 12 h; Inert atmosphereReflux;
参考文献
Chau, Nguyet Trang Thanh; Meyer, Maxime; Komagawa, Shinsuke; Chevallier, Floris; Fort, Yves; Uchiyama, Masanobu; Mongin, Florence; Gros, Philippe C.
Chemistry - A European Journal, 2010 , vol. 16, # 41 p. 12425 - 12433
696-62-8
4-碘苯甲醚
+
651358-83-7
6-溴吡啶-2-硼酸频哪酯 2-溴-6-吡啶硼酸频呐醇酯
→
反应条件
193344-39-7
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in water; N,N-dimethyl-formamide T=85°C; Suzuki cross-coupling;
参考文献
Bouillon, Alexandre; Lancelot, Jean-Charles; Santos, Jana Sopkova De Oliveira; Collot, Valerie; Bovy, Philipppe R.; Rault, Sylvain
Tetrahedron, 2003 , vol. 59, # 50 p. 10043 - 10049
696-62-8
4-碘苯甲醚
+
440680-34-2
6-溴吡啶-2-硼酸
→
反应条件
193344-39-7
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether; water Suzuki cross-coupling; Heating;
参考文献
Bouillon, Alexandre; Lancelot, Jean-Charles; Santos, Jana Sopkova De Oliveira; Collot, Valerie; Bovy, Philipppe R.; Rault, Sylvain
Tetrahedron, 2003 , vol. 59, # 50 p. 10043 - 10049
696-62-8
4-碘苯甲醚
→
反应条件
193344-39-7
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethanol; water; toluene Suzuki cross-coupling; Heating;
参考文献
Bouillon, Alexandre; Lancelot, Jean-Charles; Santos, Jana Sopkova De Oliveira; Collot, Valerie; Bovy, Philipppe R.; Rault, Sylvain
Tetrahedron, 2003 , vol. 59, # 50 p. 10043 - 10049
696-62-8
4-碘苯甲醚
→
反应条件
218608-73-2
反应条件
1: 50 percent / CuI; t-BuOK; 2,2'-bipyridyl / toluene / 4 h / Heating 2: 85 percent / PhI(O2CCF3)2; I2 / CHCl3 3: CuI; Cl2Pd(PPh3)2; TEA 4: K2CO3 / methanol View Scheme
参考文献
Planells, Miquel; Abate, Antonio; Hollman, Derek J.; Stranks, Samuel D.; Bharti, Vishal; Gaur, Jitender; Mohanty, Dibyajyoti; Chand, Suresh; Snaith, Henry J.; Robertson, Neil
Journal of Materials Chemistry A, 2013 , vol. 1, # 23 p. 6949 - 6960
1003-31-2
+
696-62-8
4-碘苯甲醚
→
反应条件
200358-05-0
反应条件
tetrabutylammomium bromide; potassium carbonate; palladium diacetate in water; acetonitrile T=80°C; 4 h;
参考文献
Gozzi, Christel; Lavenot, Laurence; Ilg, Kerstin; Penalva, Vincent; Lemaire, Marc
Tetrahedron Letters, 1997 , vol. 38, # 51 p. 8867 - 8870
1003-31-2
+
696-62-8
4-碘苯甲醚
→
反应条件
2132-80-1
+
200358-05-0
反应条件
potassium carbonate; palladium diacetate; tetrabutylammomium bromide in water; acetonitrile T=80°C; 4 h;
参考文献
Lavenot; Gozzi; Ilg; Orlova; Penalva; Lemaire
Journal of Organometallic Chemistry, 1998 , vol. 567, # 1-2 p. 49 - 55
71-23-8
+
696-62-8
4-碘苯甲醚
→
反应条件
20743-94-6
反应条件
caesium carbonate; [Cu8(S2P(OiPr)2)6(μ8-Cl)][PF6] T=110°C; 11 h;
参考文献
Manbeck, Gerald F.; Lipman, Adam J.; Stockland Jr., Robert A.; Freidl, Adrienne L.; Hasler, Amy F.; Stone, Joshua J.; Guzei, Ilia A.
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 244 - 250
696-62-8
4-碘苯甲醚
+
122-39-4
→
反应条件
反应条件
1: potassium tert-butylate; [2,2']bipyridinyl; copper(l) iodide / toluene / 24 h / 100 °C / |Inert atmosphere; |Sealed tube 2: Cu(I)[(CH3CN)4]BF4; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; 2,9-dimethyl-1,10-phenanthroline; iodine; methyloxirane / tetrahydrofuran / 20 h / 20 °C / |Flow reactor; |Inert atmosphere; |Irradiation View Scheme
参考文献
Hernandez-Perez, Augusto C.; Collins, Shawn K.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 48 p. 12696 - 12700
Angew. Chem., 2013 , vol. 125, # 48 p. 12928 - 12932
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