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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘苯甲醚
合成路线
（共 1687 条）
696-62-8
4-碘苯甲醚
+
960-16-7
三丁基苯基锡
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
potassium fluoride; 1,4-dicyclohexyl-diazabutadiene; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane T=100°C; Stille cross-coupling reaction; 16 h;
参考文献
Li, Jin-Heng; Liang, Yun; Xie, Ye-Xiang
Tetrahedron, 2005 , vol. 61, # 30 p. 7289 - 7293
696-62-8
4-碘苯甲醚
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
N-ethyl-N,N-diisopropylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in water; isopropyl alcohol T=100°C; Suzuki coupling; 0.166667 h; microwave irradiation;
参考文献
Kabalka, George W.; Al-Masum, Mohammad
Tetrahedron Letters, 2005 , vol. 46, # 37 p. 6329 - 6331
696-62-8
4-碘苯甲醚
+
934-56-5
三甲基(苯基)锡
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
potassium carbonate; Co0.38Fe0.57LaO3Pd0.05 in water T=100°C; Stille Coupling; 1 h; Product distribution / selectivity;
参考文献
Ley, Steven V.; Smith, Martin D.; Ramarao, Chandrashekar; Stepan, Antonia F.; Tanaka, Hirohisa
Patent: US2005/215804 A1, 2005 ;
Location in patent: Page/Page column 18-19 ;
696-62-8
4-碘苯甲醚
+
639-58-7
三苯基氯化锡
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
potassium acetate; palladium dichloride T=110°C; Stille Cross Coupling; 1.5 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Davan, Elham Etemadi; Rostami, Abed; Nematollahi, Arash
Journal of Organometallic Chemistry, 2013 , vol. 740, p. 123 - 130
591-50-4
碘苯
+
696-62-8
4-碘苯甲醚
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
1: para-iodoanisole With 1,1'-bis-(diphenylphosphino)ferrocene; tri(2-furyl)germane; caesium carbonate; palladium diacetate in N,N-dimethyl-formamide T=20°C; 1 h; 2: iodobenzene With tetrabutyl ammonium fluoride in tetrahydrofuran; N,N-dimethyl-formamide T=100°C; 10 h; Further stages.;
参考文献
Nakamura, Tomoaki; Kinoshita, Hidenori; Shinokubo, Hiroshi; Oshima, Koichiro
Organic Letters, 2002 , vol. 4, # 18 p. 3165 - 3167
108-86-1
溴代苯
+
696-62-8
4-碘苯甲醚
→
反应条件
92-52-4
联苯
+
613-37-6
4-甲氧基联苯
反应条件
1: bromobenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; Negishi coupling reaction; 0.166667 h; Inert atmosphere; 2: With zinc(II) chloride in tetrahydrofuran; hexane T=-78 - 20°C; Negishi coupling reaction; Inert atmosphere; 3: para-iodoanisole With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran; hexane T=60°C; Negishi coupling reaction; 2 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 131, # 29 p. 10201 - 10210
696-62-8
4-碘苯甲醚
+
71-43-2
苯
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
potassium tert-butylate T=100°C; 36 h; Inert atmosphere; chemoselective reaction;
参考文献
Zhao, Huaiqing; Shen, Jie; Guo, Juanjuan; Ye, Ruijuan; Zeng, Huaqiang
Chemical Communications, 2013 , vol. 49, # 23 p. 2323 - 2325
696-62-8
4-碘苯甲醚
+
591-51-5
苯基锂
→
反应条件
613-37-6
4-甲氧基联苯
+
2132-80-1
4,4-二甲氧基联苯
反应条件
1: phenyllithium With 1,1-dimethyl-1,3-dihydrobenzo[c][1,2]oxasilole in tetrahydrofuran T=20°C; 2 h; 2: para-iodoanisole With copper(l) iodide; palladium dichloride in tetrahydrofuran T=50°C; 2 h; Reagent/catalystTemperature;
参考文献
Martinez-Solorio, Dionicio; Hoye, Adam T.; Nguyen, Minh H.; Smith, Amos B.
Organic Letters, 2013 , vol. 15, # 10 p. 2454 - 2457
696-62-8
4-碘苯甲醚
+
603-33-8
三苯基铋
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
potassium fluoride in dimethyl sulfoxide T=105°C; 0.833333 h;
参考文献
Monguchi, Yasunari; Hattori, Tomohiro; Miyamoto, Yasuhiro; Yanase, Takayoshi; Sawama, Yoshinari; Sajiki, Hironao
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2561 - 2567
696-62-8
4-碘苯甲醚
+
1613-66-7
二苯基二氯化锗
→
反应条件
613-37-6
4-甲氧基联苯
+
2132-80-1
4,4-二甲氧基联苯
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in tetrahydrofuran; water; toluene T=115°C; 12 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 12, # 4 p. 816 - 819
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