(S)-N-Boc-吡咯烷-2-甲醛 N-(叔丁氧羰基)-L-脯氨醛合成路线 （共 52 条）
反应条件
lithium aluminium tetrahydride T=0°C; 0.25 h;
参考文献
Falkiewicz; Wisniowski; Kolodziejczyk; Wisniewski
Nucleosides, Nucleotides and Nucleic Acids, 2001 , vol. 20, # 4-7 p. 1393 - 1397
反应条件
oxalyl dichloride; dimethyl sulfoxide in triethylamine
参考文献
Ikeda, Masazumi; Shikaura, Jiro; Maekawa, Noriko; Daibuzono, Kaori; Teranishi, Hirotaka; Teraoka, Yoshiko; Oda, Norio; Ishibashi, Hiroyuki
Heterocycles, 1999 , vol. 50, # 1 p. 31 - 34
反应条件
diisobutylaluminium hydride in toluene T=-60°C; 2 h;
参考文献
McNulty; Still
Tetrahedron Letters, 1991 , vol. 32, # 37 p. 4875 - 4878
反应条件
triethylsilane; palladium on activated charcoal in acetone T=20°C;
参考文献
Tokuyama, Hidetoshi; Yokoshima, Satoshi; Lin, Shao-Cheng; Li, Leping; Fukuyama, Tohru
Synthesis, 2002 , # 8 p. 1121 - 1123
反应条件
diisobutylaluminium hydride T=-78°C;
参考文献
Coelho, Fernando; Diaz, Gaspar; Abella, Carlos A. M.; Almeida, Wanda P.
Synlett, 2006 , # 3 p. 435 - 439
反应条件
hydrogen; RhH(CO)(triphenylphosphine)3; (-)-DIPHOL in benzene T=52°C; P=25857.4 Torr; 192 h; Yield given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 45, # 11 p. 2145 - 2151
反应条件
1: BH3*THF 2: PDC View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 14 p. 2985 - 2988
反应条件
diisobutylaluminium hydride in diethyl ether; water; toluene
反应条件
triethylamine in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; dimethyl sulfoxide
反应条件
1: NaHCO3 / sonification 2: N,N'-diisopropylcarbodiimide; DMAP / CH2Cl2 3: 90 percent / DIBAL-H / -78 °C View Scheme
参考文献
Synlett, , # 3 p. 435 - 439
