反式-巴豆基硼酸频哪醇酯合成路线 （共 22 条）
反应条件
1: [Rh(nbd)(CH3CN)2]SbF6; bis(1,1-diphenylphosphino)methane / 1,2-dichloro-ethane / 0.33 h / 90 °C / Inert atmosphere
2: [Rh(nbd)(CH3CN)2]SbF6; bis(1,1-diphenylphosphino)methane / 1,2-dichloro-ethane / 6 h / 90 °C / Inert atmosphere
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参考文献
Shimizu, Hiroshi; Igarashi, Tomohiro; Miura, Tomoya; Murakami, Masahiro
Angewandte Chemie - International Edition, 2011 , vol. 50, # 48 p. 11465 - 11469
反应条件
1: bis(cyclohexanyl)borane / neat (no solvent) / 6 h / -78 - 0 °C / |Glovebox; |Inert atmosphere
2: tri-cyclo-hexyl-phosphine; [Ir(cod)2]BF4; C44H45O4P; hydrogen / 1,2-dichloro-ethane / 5.33 h / 28 °C / |Molecular sieve
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参考文献
Miura, Tomoya; Nishida, Yui; Morimoto, Masao; Murakami, Masahiro
Journal of the American Chemical Society, 2013 , vol. 135, # 31 p. 11497 - 11500
