a-[(4-羟基苯基)亚甲基]-苯乙酸合成路线 （共 5 条）
反应条件
boron trichloride in dichloromethane
T=-78 - 25°C;
参考文献
Solladie, Guy; Pasturel-Jacope, Yacine; Maignan, Jean
Tetrahedron, 2003 , vol. 59, # 18 p. 3315 - 3321
参考文献
Buckles et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 4972
View citing articles Show Details
Crawford; Moore
Journal of the Chemical Society, 1955 , p. 3445,3448
反应条件
1: 82 percent / K2CO3 / dimethylformamide / 2.5 h / 55 °C
2: 58 percent / acetic anhydride; Et3N / 12 h / 110 °C
3: 89 percent / BCl3 / CH2Cl2 / -78 - 25 °C
View Scheme
参考文献
Solladie, Guy; Pasturel-Jacope, Yacine; Maignan, Jean
Tetrahedron, 2003 , vol. 59, # 18 p. 3315 - 3321
反应条件
1: 58 percent / acetic anhydride; Et3N / 12 h / 110 °C
2: 89 percent / BCl3 / CH2Cl2 / -78 - 25 °C
View Scheme
参考文献
Solladie, Guy; Pasturel-Jacope, Yacine; Maignan, Jean
Tetrahedron, 2003 , vol. 59, # 18 p. 3315 - 3321
参考文献
Crawford; Moore
Journal of the Chemical Society, 1955 , p. 3445,3448
