1-(2-甲氧基乙基)-4-硝基苯合成路线 （共 7 条）
反应条件
hydrogen; palladium 10 on activated carbon in methanol P=760.051 Torr;
参考文献
IMOTEP INC.
Patent: WO2004/106292 A1, 2004 ;
Location in patent: Page 62 ;
反应条件
1: 2-(4-nitrophenyl)-ethanol With sodium hydride in tetrahydrofuran
T=0°C; 0.166667 h;
2: methyl iodide in tetrahydrofuran
T=20°C; 24 h;
参考文献
IMOTEP INC.
Patent: WO2004/106291 A1, 2004 ;
Location in patent: Page 59 ;
反应条件
Amberlyst 15
12 h; Reflux;
参考文献
Barontini; Proietti Silvestri; Nardi; Bovicelli; Pari; Gallucci; Spezia; Righi
Tetrahedron Letters, 2013 , vol. 54, # 37 p. 5004 - 5006
反应条件
triethylsilane; trimethylsilyl trifluoromethanesulfonate; titanium tetrachloride in dichloromethane
T=20°C; 20 h;
参考文献
Yato; Homma; Ishida
Tetrahedron, 2001 , vol. 57, # 25 p. 5353 - 5359
反应条件
potassium carbonate in acetone
24 h; Heating / reflux;
参考文献
Player, Mark R.; Parsons, William H.; Huang, Hui; Hutta, Daniel A.; Hu, Huaping; Rinker, James
Patent: US2008/114007 A1, 2008 ;
Location in patent: Page/Page column 94-95 ;
反应条件
nitric acid in dichloromethane
24 h; Ambient temperature;
参考文献
Strazzolini, Paolo; Giumanini, Angelo G.; Runcio, Antonio; Scuccato, Massimo
Journal of Organic Chemistry, 1998 , vol. 63, # 4 p. 952 - 958
反应条件
sulfuric acid; nitric acid
参考文献
CIBA
Patent: US2686806 , 1952 ;
