2-苯甲酰基-1,3-环己二酮合成路线 （共 10 条）
反应条件
potassium carbonate in water; acetonitrile
参考文献
Zeneca Limited
Patent: US6218579 B1, 2001 ;
反应条件
Sm(III) chloride; triethylamine in toluene
T=20°C; 1 h;
参考文献
Shen, Quansheng; Huang, Wen; Wang, Jialiang; Zhou, Xigeng
Organic Letters, 2007 , vol. 9, # 22 p. 4491 - 4494
参考文献
Wojtkowski, Paul Walter
Patent: US2002/49317 A1, 2002 ;
反应条件
aluminium trichloride in 1,2-dichloro-ethane
参考文献
Akhrem,A.A. et al.
Synthesis, 1978 , p. 925 - 927
反应条件
1: Et3N / CH2Cl2
2: KCN / CH2Cl2
View Scheme
参考文献
Lin, Yung-Lung; Wu, Chung-Shieh; Lin, Shean-Woei; Yang, Ding-Yah
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 9 p. 843 - 845
反应条件
1: Et3N / CH2Cl2
2: KCN / CH2Cl2
View Scheme
参考文献
Lin, Yung-Lung; Wu, Chung-Shieh; Lin, Shean-Woei; Yang, Ding-Yah
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 9 p. 843 - 845
反应条件
1: 76 percent / oxalyl chloride / 3 h / 0 °C
2: NaH / benzene / 2.5 h / 60 °C / Heating
3: p-TsOH / benzene / 10 h / Heating
View Scheme
参考文献
Tamura, Yasumitsu; Wada, Akimori; Okuyama, Shigehiro; Fukumori, Satoshi; Hayashi, Yoko; et al.
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1312 - 1320
反应条件
1: 89 percent / hydrazine / ethanol / 4 h
2: 85 percent / NaBH4 / ethanol / 6 h
View Scheme
参考文献
Croce, Piero Dalla; Rosa, Concetta La
Synthesis, 1984 , # 11 p. 982 - 983
参考文献
MITSUI PETROCHEMICAL INDUSTRIES, LTD.
Patent: EP331422 A3, 1991 ;
反应条件
bis(trichloromethyl) carbonate in 1,2-dichloro-ethane
Vilsmeier reaction; Cooling with iceReflux;
参考文献
Liang; Shi; Chen; Su
Organic Preparations and Procedures International, 2010 , vol. 42, # 4 p. 379 - 385
