反应条件
1: 1.) sodium bisulfite / 1.) ether, water, 10 deg C, 2 h, 2.) ether, water, RT, 5 h
2: 1.) t-BuOCl, 2.) Et3N / 1.) benzene, 5 deg C, 30 min, 2.) benzene, 5 deg C to RT, 4 h
3: 73 percent / AgF / acetonitrile / 15 h / 25 °C
View Scheme
参考文献
Padwa, Albert; Gasdaska, John R.; Haffmanns, Gunter; Rebello, Hector
Journal of Organic Chemistry, 1987 , vol. 52, # 6 p. 1027 - 1035
