2,6-二溴-4-甲基苯胺合成路线 （共 46 条）
参考文献
Loefgren; Lundquist
Svensk Kemisk Tidskrift, 1946 , vol. 58, p. 206,211
反应条件
1: (i) aq. HCl, NaNO2, (ii) aq. (EtOCS2)2Ca
2: aq. H2SO4
View Scheme
参考文献
Stoyanovich,F.M. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1976 , vol. 25, p. 2362 - 2367
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1976 , vol. 25, # 11 p. 2537 - 2543
反应条件
1: (i) aq. HCl, NaNO2, (ii) aq. (EtOCS2)2Ca
2: aq. H2SO4
3: aq. H2O2, AcOH
View Scheme
参考文献
Stoyanovich,F.M. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1976 , vol. 25, p. 2362 - 2367
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1976 , vol. 25, # 11 p. 2537 - 2543
参考文献
Raiford; Taft; Lankelma
Journal of the American Chemical Society, 1924 , vol. 46, p. 2056
反应条件
1: (i) aq. HCl, NaNO2, (ii) aq. (EtOCS2)2Ca
2: aq. H2SO4
3: aq. H2O2, AcOH
4: (i) nBuLi, (ii) H2O
View Scheme
参考文献
Stoyanovich,F.M. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1976 , vol. 25, p. 2362 - 2367
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1976 , vol. 25, # 11 p. 2537 - 2543
反应条件
1: Diazotization.Behandlung der Diazoniumsalz-Loesung mit CuBr in wss. HBr
2: bromine / 200 - 220 °C / Erhitzen des Reaktionsprodukts mit konz. Schwefelsaeure auf 150grad
View Scheme
参考文献
Asinger
Journal fuer Praktische Chemie (Leipzig), 1935 , vol. <2> 142, p. 291,299
