1-乙酰氨基丙烷-1,1,3-三羧酸三乙酯合成路线 （共 12 条）
反应条件
hydrogenchloride T=90 - 100°C; 16 h;
参考文献
Angell, Paul; Blazecka, Peter G.; Lovdahl, Mark; Zhang, Ji
Journal of Organic Chemistry, 2007 , vol. 72, # 17 p. 6606 - 6609
参考文献
Kato et al.
Nippon Nogei Kagaku Kaishi, 1953 , vol. 27, p. 500
Chem.Abstr., 1955 , p. 3006
Full Text Show Details
Talbot et al.
Canadian Journal of Chemistry, 1956 , vol. 34, p. 1440,1441
反应条件
1: ethanolic sodium ethylate 2: ethanolic KOH 3: 150 - 160 °C View Scheme
参考文献
Cocolas; Hartung
Journal of the American Chemical Society, 1957 , vol. 79, p. 5203
反应条件
hydrogen; palladium on activated charcoal in ethanol
T=20 - 25°C; P=2585.81 Torr; 1 h;
参考文献
Angell, Paul; Blazecka, Peter G.; Lovdahl, Mark; Zhang, Ji
Journal of Organic Chemistry, 2007 , vol. 72, # 17 p. 6606 - 6609
反应条件
1: 38 percent / indium(III) triflate; N-methylmorpholine / 26 h / 120 - 130 °C
2: 100 percent / H2 / Pd on carbon / ethanol / 1 h / 20 - 25 °C / 2585.81 Torr
View Scheme
参考文献
Angell, Paul; Blazecka, Peter G.; Lovdahl, Mark; Zhang, Ji
Journal of Organic Chemistry, 2007 , vol. 72, # 17 p. 6606 - 6609
反应条件
1: 38 percent / indium(III) triflate; N-methylmorpholine / 26 h / 120 - 130 °C
2: 100 percent / H2 / Pd on carbon / ethanol / 1 h / 20 - 25 °C / 2585.81 Torr
View Scheme
参考文献
Angell, Paul; Blazecka, Peter G.; Lovdahl, Mark; Zhang, Ji
Journal of Organic Chemistry, 2007 , vol. 72, # 17 p. 6606 - 6609
参考文献
Cocolas; Hartung
Journal of the American Chemical Society, 1957 , vol. 79, p. 5203
反应条件
hydrogen; platinum(IV) oxide in ethanol
参考文献
Kishida,Y.; Nakamura,N.
Chemical and Pharmaceutical Bulletin, 1969 , vol. 17, p. 2424 - 2435
反应条件
1: (i) KOtBu, tBuOH, (ii) /BRN= 1904574/
2: H2 / PtO2 / ethanol
View Scheme
参考文献
Kishida,Y.; Nakamura,N.
Chemical and Pharmaceutical Bulletin, 1969 , vol. 17, p. 2424 - 2435
参考文献
Talbot et al.
Canadian Journal of Chemistry, 1956 , vol. 34, p. 1440,1441
