四氟乙烷-beta-磺内酯合成路线 (共 50 条)
反应条件
at -10°C, in teflon reactor, 6 h, water free HCl used;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
反应条件
in diethyl ether at 10°C;
参考文献
England,D.C. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 6181 - 6188
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Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
参考文献
Dmitriev, M. A.; Sokol'skii, G. A.; Knunyants, I. L.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , p. 1137 - 1140
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , p. 1227 - 1230
C.A., 1961 , p. 2544
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 972 - 976
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 1017 - 1022
C.A., , vol. 65, p. 10486
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
参考文献
Belaventzev,M.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1967 , p. 2344 - 2347
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 2461 - 2465
反应条件
in neat (no solvent) ice cooling;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
反应条件
silver fluoride 1.) diglyme, 3h, 35 deg C, 2.) 35 deg C, 3 d; Yield given. Multistep reaction;
参考文献
Chen, Li-Fo; Mohtasham, Javid; Gard, Gary L.
Journal of Fluorine Chemistry, 1990 , vol. 49, # 3 p. 331 - 347
反应条件
silver fluoride 1.) diglyme, -196 deg C, then 1.5 h at 35 deg C; 2.) -196 deg C, then 3 d at 35 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chen, Li-Fo; Mohtasham, Javid; Gard, Gary L.
Journal of Fluorine Chemistry, 1990 , vol. 46, # 1 p. 39 - 56
反应条件
silver fluoride 1.) diglyme, -196 deg C, then 2 h at 30-35 deg C; 2.) toluene, -196 deg C, then 2 h at 5-8 deg C and 16 h at 18-20 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chen, Li-Fo; Mohtasham, Javid; Gard, Gary L.
Journal of Fluorine Chemistry, 1990 , vol. 46, # 1 p. 39 - 56