四氟乙烷-beta-磺内酯合成路线 （共 50 条）
反应条件
silver fluoride multistep reaction : new polyfluoroalkoxysulfonyl fluorides; competition reaction with o-(CF3)2C6H3CH2Br, C6F5CH2Br;
参考文献
Chen, Li-Fo; Mohtasham, Javid; Gard, Gary L.
Journal of Fluorine Chemistry, 1990 , vol. 49, # 3 p. 331 - 347
反应条件
warming on water bath under reflux, at 40-50°C, 2-3 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
反应条件
silver fluoride 1.) diglyme, -196 deg C, then 1.5 h at 35 deg C; 2.) -196 deg C, then 3 d at 35 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chen, Li-Fo; Mohtasham, Javid; Gard, Gary L.
Journal of Fluorine Chemistry, 1990 , vol. 46, # 1 p. 39 - 56
反应条件
warming on water bath under reflux, at 30-40°C, 1 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
参考文献
Knunyants, I. L.; Sokol'skii, G. A.; Belaventsev, M. A.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1966 , p. 977 - 980
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1966 , p. 1022 - 1027
C.A., 1966 , vol. 65, p. 10486
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
参考文献
Knunyants, I. L.; Sokol'skii, G. A.; Belaventsev, M. A.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1966 , p. 977 - 980
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1966 , p. 1022 - 1027
C.A., 1966 , vol. 65, p. 10486
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
反应条件
sulfuric acid byproducts: CO; heating, 100 percent H2SO4;
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2070 - 2073
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2220 - 2224
C.A., , vol. 77, p. 42670
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 1935 - 1938
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2020 - 2024
C.A., , vol. 68, p. 39564
反应条件
abs. ethylene used, at 35-40°C;
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 574 - 578
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 625 - 630
反应条件
at -10°C, in teflon reactor, 6 h, water free HCl used;
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 574 - 578
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 625 - 630
