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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
R-(-)-1-茚酚
合成路线
（共 59 条）
6351-10-6
1-羟基茚满
+
182877-84-5
→
反应条件
697-64-3
R-(-)-1-茚酚
+
25501-32-0
(S)-(+)-1-茚醇
反应条件
methylmagnesium bromide in dichloromethane T=0°C; Acylation; 2 h; Product distribution; Further Variations:SolventsTemperaturesReagents;
参考文献
Journal of Organic Chemistry, , vol. 64, # 26 p. 9365 - 9373
918442-98-5
→
反应条件
697-64-3
R-(-)-1-茚酚
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride
参考文献
Tetrahedron Asymmetry, , vol. 17, # 18 p. 2713 - 2721
6351-10-6
1-羟基茚满
+
123-62-6
丙酸酐
→
反应条件
反应条件
(S)-(-)-BTM; sodium sulfate; N-ethyl-N,N-diisopropylamine in chloroform T=20°C; 22 h; Resolution of racemate; Kinetics; Reagent/catalyst; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 77, # 4 p. 1722 - 1737
123-20-6
正丁酸乙烯酯
+
6351-10-6
1-羟基茚满
→
反应条件
697-64-3
R-(-)-1-茚酚
+
25501-32-0
(S)-(+)-1-茚醇
+
158529-97-6
反应条件
in benzene T=35°C; 2.5 h; Irradiationporcine pancreas lipase-catalyzed; microwave irradiation; ee investigated; Rate constantProduct distribution;
参考文献
Tetrahedron Letters, , vol. 39, # 24 p. 4333 - 4336
6351-10-6
1-羟基茚满
+
57-10-3
棕榈酸
→
反应条件
697-64-3
R-(-)-1-茚酚
+
25501-32-0
(S)-(+)-1-茚醇
反应条件
in benzene 2.5 h; HeatingIrradiationporcine pancreas lipase-catalyzed; microwave irradiation; ee investigated; Rate constantProduct distribution;
参考文献
Tetrahedron Letters, , vol. 39, # 24 p. 4333 - 4336
697-64-3
R-(-)-1-茚酚
→
反应条件
83-33-0
1-茚酮
反应条件
Lactobacillus kefir alcohol dehydrogenase; tris(hydroxymethyl)methylamine hydrochloride; NADPH in water T=30°C; pH=7; 0.25 h; aq. bufferEnzymatic reaction;
参考文献
Endo, Satoshi; Matsunaga, Toshiyuki; Matsumoto, Atsuko; Arai, Yuki; Ohno, Satoshi; El-Kabbani, Ossama; Tajima, Kazuo; Bunai, Yasuo; Yamano, Shigeru; Hara, Akira; Kitade, Yukio
Biochemical Pharmacology, 2013 , vol. 86, # 9 p. 1366 - 1375
697-64-3
R-(-)-1-茚酚
→
反应条件
6351-10-6
1-羟基茚满
+
83-33-0
1-茚酮
反应条件
[Ir(η5-C5Me5)(C6H4-2-CH2NHCH3)(NCCH3)](PF6); potassium tert-butylate in toluene T=20°C; 24 h; Inert atmosphere;
参考文献
Jerphagnon, Thomas; Gayet, Arnaud J.A.; Berthiol, Florian; Ritleng, Vincent; Mrsic, Natasa; Meetsma, Auke; Pfeffer, Michel; Minnaard, Adriaan J.; Feringa, Ben L.; De Vries, Johannes G.
Chemistry - A European Journal, 2009 , vol. 15, # 46 p. 12780 - 12790
697-64-3
R-(-)-1-茚酚
→
反应条件
6351-10-6
1-羟基茚满
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; N,N'-methyl-(3-dimethylaminopropyl)-amine in toluene T=80°C; 5 h;
参考文献
Riermeier, Thomas H.; Gross, Peter; Monsees, Axel; Hoff, Manfred; Trauthwein, Harald
Tetrahedron Letters, 2005 , vol. 46, # 19 p. 3403 - 3406
697-64-3
R-(-)-1-茚酚
→
反应条件
6351-10-6
1-羟基茚满
+
83-33-0
1-茚酮
反应条件
[Ir(η5-C5Me5)(C6H4-2-CH2NHCH3)(NCCH3)](PF6); potassium tert-butylate in toluene T=20°C; 24 h; Inert atmosphere;
参考文献
Jerphagnon, Thomas; Gayet, Arnaud J.A.; Berthiol, Florian; Ritleng, Vincent; Mrsic, Natasa; Meetsma, Auke; Pfeffer, Michel; Minnaard, Adriaan J.; Feringa, Ben L.; De Vries, Johannes G.
Chemistry - A European Journal, 2009 , vol. 15, # 46 p. 12780 - 12790
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