2,3,5-三甲基苯酚合成路线 (共 124 条)
反应条件
titanium(III) chloride; lithium in tetrahydrofuran T=25°C; Substitution; 18 h;
参考文献
Nayak
Synthesis, 2000 , # 11 p. 1575 - 1578
反应条件
calcium hydroxide powder
参考文献
Journal of the Chemical Society, , p. 400,403
反应条件
1,4-dioxane; copper oxide-chromium oxide T=165°C; Hydrogenolyse;
参考文献
Journal of the American Chemical Society, , vol. 61, p. 765
反应条件
1,4-dioxane; copper oxide-chromium oxide T=165°C; Hydrogenolyse;
参考文献
Journal of the American Chemical Society, , vol. 61, p. 765
反应条件
aluminium trichloride
参考文献
Karpf, Martin
Helvetica Chimica Acta, 1984 , vol. 67, # 1 p. 73 - 85
反应条件
sulfuric acid T=20°C;
参考文献
Journal of the American Chemical Society, , vol. 71, p. 2221,2224
反应条件
diethylzinc in toluene 1.5 h; Heating;
参考文献
Lehnert, Erich K.; Sawyer, J. Scott; Macdonald, Timothy L.
Tetrahedron Letters, 1989 , vol. 30, # 39 p. 5215 - 5218
反应条件
1: With 10 Pd/C in ethylene glycol 6 h; Inert atmosphereReflux; 2: With hydrogenchloride in water; ethylene glycol Inert atmosphere;
参考文献
Majetich, George; Allen, Scott
Arkivoc, 2010 , vol. 2010, # 4 p. 104 - 124
反应条件
in tetrahydrofuran; dimethyl sulfoxide 1.) -5 deg C, 1 h, 2.) room temperature, 7 h;
参考文献
Garst, Michael E.; Frazier, Janice D.
Journal of Organic Chemistry, 1982 , vol. 47, # 18 p. 3553 - 3556
反应条件
10 Pd/C in ethylene glycol 6 h; Inert atmosphereReflux;
参考文献
Majetich, George; Allen, Scott
Arkivoc, 2010 , vol. 2010, # 4 p. 104 - 124