4-溴-2,6-二氯苯胺合成路线 (共 17 条)
反应条件
Iodine bromide; acetic acid
参考文献
Ferguson, George; Low, John N.; Penner, Glenn H.; Wardell, James L.
Acta Crystallographica Section C: Crystal Structure Communications, 1998 , vol. 54, # 12 p. 1974 - 1977
反应条件
1.1: 82 percent / Na2CO3 / Pd(PPh3)4 / toluene; ethanol / 14 h / 80 °C / Formation of xenobiotics 2.1: H2SO4; NaNO2 2.2: 42 percent / CuCl / Formation of xenobiotics View Scheme
参考文献
Lehmler, Hans-Joachim; Robertson, Larry W
Chemosphere, 2001 , vol. 45, # 2 p. 137 - 143
反应条件
sulfuric acid in acetic acid T=20°C; 1 h;
参考文献
Hanson, James R.; Saberi, Hamid
Journal of Chemical Research, 2004 , # 10 p. 699 - 701
参考文献
Reed; Orton
Journal of the Chemical Society, 1907 , vol. 91, p. 1553
反应条件
hydrogen bromide; acetic acid; aniline 24 h; Heating;
参考文献
Choi; Chi
Journal of the American Chemical Society, 2001 , vol. 123, # 37 p. 9202 - 9203
反应条件
potassium iodide; sulfuric acid; sodium thiosulfate; sodium nitrite in ice-water
参考文献
JAPAN POLYPROPYLENE CORPORATION
Patent: US2005/70426 A1, 2005 ;
反应条件
sulfuric acid; acetic acid; potassium iodide; sodium nitrite
1.)0-5 deg C; 2.)heated; Yield given. Multistep reaction;
参考文献
Prasad, M. Arun; Sangaranarayanan
Tetrahedron, 2004 , vol. 60, # 48 p. 10967 - 10972