3,4,5-三乙氧基苯甲酸合成路线 （共 11 条）
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 51, # 9 p. 1085 - 1088
反应条件
1: K2CO3; KI / acetone / 48 h / Heating 2: aq. KOH / ethanol / 4 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 3 p. 888 - 903
反应条件
sodium hydroxide anschliessendes Erwaermen mit wss. Natronlauge;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 137, p. 339,349
Archiv der Pharmazie (Weinheim, Germany), , vol. 272, p. 221,235
反应条件
1: TsOH / toluene 2: K2CO3 / dimethylformamide 3: aq. KOH View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 51, # 9 p. 1085 - 1088
参考文献
Journal of the Chemical Society, , vol. 81, p. 205
参考文献
Sugihara,H. et al.
Justus Liebigs Annalen der Chemie, 1972 , vol. 763, p. 109 - 120
反应条件
1: thionyl chloride
2: xylene; palladium/barium sulfate / 150 °C / Hydrogenation
3: ethanol; aqueous methanol. KOH / unter Kuehlung
4: acetic acid; ethanol; aqueous hydrochloric acid / Reduktion an Blei-Kathoden
View Scheme
参考文献
Slotta; Szyszka
Journal fuer Praktische Chemie (Leipzig), 1933 , vol. <2> 137, p. 339,349
反应条件
alkali hydroxide
in waessr. oder alkoh. Loesung unter Druck;
参考文献
Basler Chem. Fabr.
Patent: DE162658 ;
反应条件
1: H2SO4 / Ambient temperature
2: (i) aq. NaOH, (ii) /BRN= 635994/, (iii) aq. NaOH
View Scheme
参考文献
Ernest,I. et al.
Collection of Czechoslovak Chemical Communications, 1963 , vol. 28, p. 1022 - 1030
反应条件
1: sulfuric acid
2: hydrazine hydrate
View Scheme
参考文献
Feist; Klatt; Awe
Archiv der Pharmazie (Weinheim, Germany), 1934 , vol. 272, p. 221,235
